tetrahydropyranyl-2-keto-6-β-propenal

Base Information

Chemical Name:tetrahydropyranyl-2-keto-6-β-propenal
CAS No.:344400-54-0
Molecular Formula:C₈H₁₀O₃
Molecular Weight:154.166
Hs Code.:

Synonyms:

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Chemical Property of tetrahydropyranyl-2-keto-6-β-propenal

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Technology Process of tetrahydropyranyl-2-keto-6-β-propenal

There total 3 articles about tetrahydropyranyl-2-keto-6-β-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78946-03-9
6-((Z)-2-[1,3]Dioxolan-2-yl-vinyl)-tetrahydro-pyran-2-one

: 344400-54-0,77803-32-8
tetrahydropyranyl-2-keto-6-β-propenal

Guidance literature:: With phosphoric acid; silica gel; In dichloromethane; for 4h;

Reference yield:

: 100-73-2
acrolein dimer

: 344400-54-0,77803-32-8
tetrahydropyranyl-2-keto-6-β-propenal

Guidance literature:: Multi-step reaction with 3 steps

1: Li / methanol; dimethylformamide / 4 h / 85 - 90 °C

2: PCC, sodium acetate / CH₂Cl₂ / 4 h / Ambient temperature

3: 85percent H₃PO₄ (SiO₂) / CH₂Cl₂ / 4 h

With phosphoric acid; sodium acetate; silica gel; lithium; pyridinium chlorochromate; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 78946-04-0
2-((Z)-2-[1,3]Dioxolan-2-yl-vinyl)-3,4-dihydro-2H-pyran

: 344400-54-0,77803-32-8
tetrahydropyranyl-2-keto-6-β-propenal

Guidance literature:: Multi-step reaction with 2 steps

1: PCC, sodium acetate / CH₂Cl₂ / 4 h / Ambient temperature

2: 85percent H₃PO₄ (SiO₂) / CH₂Cl₂ / 4 h

With phosphoric acid; sodium acetate; silica gel; pyridinium chlorochromate; In dichloromethane;