2-Acetyl-3,4-diethyl-pyrrol

Base Information

• Chemical Name: 2-Acetyl-3,4-diethyl-pyrrol
• CAS No.: 2169-20-2
• Molecular Formula: C₁₀H₁₅NO
• Molecular Weight: 165.235
• Mol file: 2169-20-2.mol

Synonyms:

Chemical Property of 2-Acetyl-3,4-diethyl-pyrrol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Acetyl-3,4-diethyl-pyrrol

There total 2 articles about 2-Acetyl-3,4-diethyl-pyrrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,4-diethyl-1H-pyrrole (16200-52-5) + N,N-dimethyl acetamide (127-19-5,116057-81-9) → 2-Acetyl-3,4-diethyl-pyrrol (2169-20-2)

Guidance literature:

N,N-dimethyl acetamide; With trichlorophosphate; at 20 ℃; for 0.25h;

3,4-diethyl-1H-pyrrole; In 1,2-dichloro-ethane; for 4h; Reflux;

With sodium acetate; In 1,2-dichloro-ethane; for 4h; Reflux;

DOI:10.1002/ejoc.201700891

Reference yield:

→ 2-Acetyl-3,4-diethyl-pyrrol (2169-20-2)

Guidance literature:

3,4-Diethyl-pyrrol, Zinkacetat-dihydrat, wss. 80percent-ig. Eg., unter Stickstoff, Erhitzen, neben 1,2,6,7-Tetraethyl-indolizin;

Reference yield: 83.0%

2-Acetyl-3,4-diethyl-pyrrol (2169-20-2) → C10H14INO

Guidance literature:

With potassium triiodide; sodium hydrogencarbonate; In water; 1,2-dichloro-ethane; at 80 ℃; for 1.5h; Inert atmosphere;

DOI:10.1002/ejoc.201700891

upstream raw materials:

3,4-diethyl-1H-pyrrole

N,N-dimethyl acetamide