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(16S)-16-methoxy-16-methyl-PGE1 methyl ester

Base Information Edit
  • Chemical Name:(16S)-16-methoxy-16-methyl-PGE1 methyl ester
  • CAS No.:76817-56-6
  • Molecular Formula:C23H40O6
  • Molecular Weight:412.567
  • Hs Code.:
  • Mol file:76817-56-6.mol
(16S)-16-methoxy-16-methyl-PGE<sub>1</sub> methyl ester

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Chemical Property of (16S)-16-methoxy-16-methyl-PGE1 methyl ester Edit
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Technology Process of (16S)-16-methoxy-16-methyl-PGE1 methyl ester

There total 10 articles about (16S)-16-methoxy-16-methyl-PGE1 methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 10 steps
1: 90 percent / Na2S2O5 / H2O / a) below 40 deg C, 30 min, b) 0 deg C, 2 h
2: 68 percent / HCl(g) / 0 - 5 °C
3: 1.) NaH / 1.) THF, 2.) THF, reflux, 30 min
4: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, -78 deg C, 2 h
5: 1.) NaH / 1.) DME, 1 h, 2.) DME, 5 h
6: 14.4 percent / NaBH4 / methanol; H2O / 2 h / -78 °C
7: p-toluenesulfonic acid / benzene / 0.5 h / Ambient temperature
8: K2CO3 / methanol / 24 h / Ambient temperature
9: pyr2*CrO3 (Collins reagent) / CH2Cl2 / 1 h
10: H2O, CH3COOH / tetrahydrofuran / 2 h / 45 °C
With hydrogenchloride; sodium metabisulfite; sodium tetrahydroborate; n-butyllithium; water; dipyridine chromium trioxide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water; benzene;
DOI:10.1021/jm00160a005
Guidance literature:
Multi-step reaction with 9 steps
1: 68 percent / HCl(g) / 0 - 5 °C
2: 1.) NaH / 1.) THF, 2.) THF, reflux, 30 min
3: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, -78 deg C, 2 h
4: 1.) NaH / 1.) DME, 1 h, 2.) DME, 5 h
5: 14.4 percent / NaBH4 / methanol; H2O / 2 h / -78 °C
6: p-toluenesulfonic acid / benzene / 0.5 h / Ambient temperature
7: K2CO3 / methanol / 24 h / Ambient temperature
8: pyr2*CrO3 (Collins reagent) / CH2Cl2 / 1 h
9: H2O, CH3COOH / tetrahydrofuran / 2 h / 45 °C
With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; water; dipyridine chromium trioxide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water; benzene;
DOI:10.1021/jm00160a005
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