(2,3,8,9-tetramethoxy-5,6-dimethyl-6H-benzo[c]phenanthridin-11-yl) acetate

Base Information

Chemical Name:(2,3,8,9-tetramethoxy-5,6-dimethyl-6H-benzo[c]phenanthridin-11-yl) acetate
CAS No.:93772-18-0
Molecular Formula:C₂₅H₂₇NO₆
Molecular Weight:437.492
Hs Code.:
ChEMBL ID:CHEMBL1996809
DSSTox Substance ID:DTXSID30409325
NSC Number:379965

Synonyms:93772-18-0;NCI60_003591;(2,3,8,9-tetramethoxy-5,6-dimethyl-6H-benzo[c]phenanthridin-11-yl) acetate;CHEMBL1996809;DTXSID30409325;NSC379965;NSC-379965

Suppliers and Price of (2,3,8,9-tetramethoxy-5,6-dimethyl-6H-benzo[c]phenanthridin-11-yl) acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of (2,3,8,9-tetramethoxy-5,6-dimethyl-6H-benzo[c]phenanthridin-11-yl) acetate

Chemical Property:

Vapor Pressure:7.57E-17mmHg at 25°C
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:6
Exact Mass:437.18383758
Heavy Atom Count:32
Complexity:660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1C2=CC(=C(C=C2C3=C(N1C)C4=CC(=C(C=C4C=C3OC(=O)C)OC)OC)OC)OC

Technology Process of (2,3,8,9-tetramethoxy-5,6-dimethyl-6H-benzo[c]phenanthridin-11-yl) acetate

There total 6 articles about (2,3,8,9-tetramethoxy-5,6-dimethyl-6H-benzo[c]phenanthridin-11-yl) acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108-24-7
acetic anhydride

: 93772-17-9
2,3,8,9-tetramethoxy-5,6-dimethyl-11-hydroxy-5,6-dihydrobenzophenanthridine hydrochloride

: 93772-18-0
2,3,8,9-tetramethoxy-5,6-dimethyl-11-acetoxy-5,6-dihydrobenzophenanthridine

Guidance literature:: With pyridine; for 0.5h; Heating;

Reference yield:

: 40940-49-6
ethyl 2-<2'-<1''-(3,4-dimethoxyphenyl)-2''-oxoethyl>-4',5'-dimethoxyphenyl>acetic acid

: 93772-18-0
2,3,8,9-tetramethoxy-5,6-dimethyl-11-acetoxy-5,6-dihydrobenzophenanthridine

Guidance literature:: Multi-step reaction with 6 steps

1: 70percent HClO₄ / 2 h / 0 °C

2: aq NH₃ / ethanol / 0.67 h / Heating

3: 3.5 g / H₂SO₄ / 24 h

4: 0.18 g / DMF / 18 h / Ambient temperature

5: 44 percent / NaBH₄ / tetrahydrofuran / 1.) 0 deg C, 20+20 min; 2.) water bath, 30 min

6: 82 percent / pyridine / 0.5 h / Heating

With pyridine; ammonium hydroxide; sodium tetrahydroborate; perchloric acid; sulfuric acid; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol;

Reference yield:

: 93772-14-6
1-methyl-3-(2-carboxymethyl-4,5-dimethoxyphenyl)-6,7-dimethoxyisoquinoline

: 93772-18-0
2,3,8,9-tetramethoxy-5,6-dimethyl-11-acetoxy-5,6-dihydrobenzophenanthridine

Guidance literature:: Multi-step reaction with 4 steps

1: 3.5 g / H₂SO₄ / 24 h

2: 0.18 g / DMF / 18 h / Ambient temperature

3: 44 percent / NaBH₄ / tetrahydrofuran / 1.) 0 deg C, 20+20 min; 2.) water bath, 30 min

4: 82 percent / pyridine / 0.5 h / Heating

With pyridine; sodium tetrahydroborate; sulfuric acid; N,N-dimethyl-formamide; In tetrahydrofuran;