4-CHLORO-2-FLUOROPHENYL CYCLOPROPYL KETONE

Base Information

• Chemical Name: 4-CHLORO-2-FLUOROPHENYL CYCLOPROPYL KETONE
• CAS No.: 898790-24-4
• Molecular Formula: C₁₀H₈ClFO
• Molecular Weight: 198.624
• Mol file: 898790-24-4.mol

Synonyms:

Chemical Property of 4-CHLORO-2-FLUOROPHENYL CYCLOPROPYL KETONE

Chemical Property:

• Vapor Pressure: 0.00345mmHg at 25°C

Purity/Quality:

97% ^*data from raw suppliers

4-chloro-2-fluorophenylcyclopropylketone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-CHLORO-2-FLUOROPHENYL CYCLOPROPYL KETONE

There total 2 articles about 4-CHLORO-2-FLUOROPHENYL CYCLOPROPYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-Chloro-2-fluorophenyl)(cyclopropyl)methanol (1202774-93-3) → C10H8ClFO (898790-24-4)

Guidance literature:

With dipyridinium dichromate; In dichloromethane; at 0 - 20 ℃; for 10h;

DOI:10.1021/acs.orglett.0c01992

Reference yield:

4-chloro-2-fluorobenzaldehyde (61072-56-8) → C10H8ClFO (898790-24-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 5 h / 0 - 20 °C

2: dipyridinium dichromate / dichloromethane / 10 h / 0 - 20 °C

With dipyridinium dichromate; In tetrahydrofuran; dichloromethane;

DOI:10.1021/acs.orglett.0c01992

upstream raw materials:

4-chloro-2-fluorobenzaldehyde

(4-Chloro-2-fluorophenyl)(cyclopropyl)methanol

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