C₁₀H₁₈O₂

Base Information

• Chemical Name: C₁₀H₁₈O₂
• CAS No.: 1254369-07-7
• Molecular Formula: C₁₀H₁₈O₂
• Molecular Weight: 170.252
• Mol file: 1254369-07-7.mol

Synonyms:

Chemical Property of C₁₀H₁₈O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₈O₂

There total 4 articles about C₁₀H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylpent-1-en-3-ol (96481-55-9,2088-07-5) → C10H18O2 (1254369-07-7)

Guidance literature:

Multi-step reaction with 5 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate

2: titanium(IV) isopropylate; Trimethylacetic acid

3: pyridinium p-toluenesulfonate

4: oxalyl dichloride; dimethyl sulfoxide; triethylamine

With titanium(IV) isopropylate; tert.-butylhydroperoxide; oxalyl dichloride; pyridinium p-toluenesulfonate; D-(-)-diisopropyl tartrate; dimethyl sulfoxide; triethylamine; Trimethylacetic acid; 1: Sharpless asymmetric epoxidation / 4: Swern oxidation / 5: Wittig methylenation;

DOI:10.1021/jo201319b

Reference yield:

4,5-dideoxy-2C-methyl-D-erythro-pentitol (108510-19-6) → C10H18O2 (1254369-07-7)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridinium p-toluenesulfonate

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine

With oxalyl dichloride; pyridinium p-toluenesulfonate; dimethyl sulfoxide; triethylamine; 2: Swern oxidation / 3: Wittig methylenation;

DOI:10.1021/jo201319b

Reference yield:

(2S,3R)-1,2-epoxy-2-methylpentan-3-ol (159170-70-4) → C10H18O2 (1254369-07-7)

Guidance literature:

Multi-step reaction with 4 steps

1: titanium(IV) isopropylate; Trimethylacetic acid

2: pyridinium p-toluenesulfonate

3: oxalyl dichloride; dimethyl sulfoxide; triethylamine

With titanium(IV) isopropylate; oxalyl dichloride; pyridinium p-toluenesulfonate; dimethyl sulfoxide; triethylamine; Trimethylacetic acid; 3: Swern oxidation / 4: Wittig methylenation;

DOI:10.1021/jo201319b

upstream raw materials:

2-methylpent-1-en-3-ol

4,5-dideoxy-2C-methyl-D-erythro-pentitol

(4R,5S) 2,2,4-trimethyl-5-ethyl-1,3-dioxolane-4-carboxaldehyde

Methylenetriphenylphosphorane