2-methyl-2-propyl-1,3-dithiolane

Base Information

• Chemical Name: 2-methyl-2-propyl-1,3-dithiolane
• CAS No.: 57230-59-8
• Molecular Formula: C7H14 S2
• Molecular Weight: 162.32
• Mol file: 57230-59-8.mol

Synonyms:

Chemical Property of 2-methyl-2-propyl-1,3-dithiolane

Chemical Property:

• Vapor Pressure: 0.182mmHg at 25°C
• Boiling Point: 218.8°Cat760mmHg
• Flash Point: 81.1°C
• Density: 1.013g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-methyl-2-propyl-1,3-dithiolane

There total 1 articles about 2-methyl-2-propyl-1,3-dithiolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethane-1,2-dithiol (540-63-6) + 2-Pentanone (107-87-9) → 2-methyl-2-propyl-1,3-dithiolane (57230-59-8)

Guidance literature:

With indium(III) bromide; In dichloromethane; at 20 ℃; for 1.2h;

DOI:10.1016/S0040-4039(00)01741-X

Reference yield: 94.0%

2-methyl-2-propyl-1,3-dithiolane (57230-59-8) → 2-Pentanone (107-87-9)

Guidance literature:

With selenium(IV) oxide; In acetic acid; for 1.16667h; Ambient temperature;

DOI:10.1055/s-1995-3842

upstream raw materials:

ethane-1,2-dithiol

2-Pentanone

Downstream raw materials:

2-Pentanone

Refernces

• 1、 Ceschi,De Araujo Felix,Peppe. "Indium tribromide-catalyzed chemoselective dithioacetalization of aldehydes in non-aqueous and aqueous media". . p. 9695 - 9699. Retrieved 2007/10/03.
• 2、 Robbe,Fernandez,Dubief,et al.. "Comparative radioprotective activity of various pentagonal compounds with two heteroatomes". . p. 235 - 243. Retrieved 2007/10/02.