3,6-dimethylcholanthrene picrate

Base Information

• Chemical Name: 3,6-dimethylcholanthrene picrate
• CAS No.: 85923-38-2
• Molecular Formula: C₆H₃N₃O₇*C₂₂H₁₈
• Molecular Weight: 511.491
• Mol file: 85923-38-2.mol

Synonyms:

Chemical Property of 3,6-dimethylcholanthrene picrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,6-dimethylcholanthrene picrate

There total 1 articles about 3,6-dimethylcholanthrene picrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6,12b-Dihydro-3,6-dimethylcholanthrene (90823-02-2) → 3,6-dimethylcholanthrene picrate (85923-38-2)

Guidance literature:

With 2,4,6-Trinitrophenol; sulfur; 1.) 160-165 deg C, 1h, 2.) benzene, hot alcohol;

DOI:10.1021/jo00162a029

Reference yield: 71.0%

3,6-dimethylcholanthrene picrate (85923-38-2) → 3,6-Dimethylcholanthrene (85923-37-1)

Guidance literature:

chromatography over basic alumina (benzene);

DOI:10.1021/jo00162a029

upstream raw materials:

6,12b-Dihydro-3,6-dimethylcholanthrene

Downstream raw materials:

3,6-Dimethylcholanthrene