Acetamide, N-[5-(diethylamino)-2-[[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-1-pyrrolidin yl)-2-propenylidene]amino]phenyl]-

Base Information

Chemical Name:Acetamide, N-[5-(diethylamino)-2-[[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-1-pyrrolidin yl)-2-propenylidene]amino]phenyl]-
CAS No.:140234-93-1
Molecular Formula:C23H23N7O3
Molecular Weight:445.47400
Hs Code.:

Synonyms:Acetamide,N-[5-(diethylamino)-2-[[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-1-pyrrolidinyl)-2-propenylidene]amino]phenyl];

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetamide, N-[5-(diethylamino)-2-[[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-1-pyrrolidin yl)-2-propenylidene]amino]phenyl]-

Chemical Property:

PSA：156.94000
Density:1.25±0.1 g/cm3(Predicted)
LogP:3.37094

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetamide, N-[5-(diethylamino)-2-[[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-1-pyrrolidin yl)-2-propenylidene]amino]phenyl]-

There total 2 articles about Acetamide, N-[5-(diethylamino)-2-[[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-1-pyrrolidin yl)-2-propenylidene]amino]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 140714-28-9
N-{2-[2-Amino-1,3,3-tricyano-prop-2-en-(Z)-ylideneamino]-5-diethylamino-phenyl}-acetamide

: 4100-80-5
2-methylsuccinic anhydride

: 140234-93-1
N-{5-Diethylamino-2-[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-pyrrolidin-1-yl)-prop-2-en-(Z)-ylideneamino]-phenyl}-acetamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1016/S0040-4039(00)91588-0

Reference yield:

: 121081-57-0
N-(5-Diethylamino-2-nitroso-phenyl)-acetamide

: 140234-93-1
N-{5-Diethylamino-2-[1,3,3-tricyano-2-(3-methyl-2,5-dioxo-pyrrolidin-1-yl)-prop-2-en-(Z)-ylideneamino]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NEt₃ / ethanol / 20 °C

2: 95 percent / NEt₃ / CH₂Cl₂ / 0.25 h / 20 °C

With triethylamine; In ethanol; dichloromethane;
DOI:10.1016/S0040-4039(00)91588-0