Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

Base Information

Chemical Name:Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester
CAS No.:77012-07-8
Molecular Formula:C₃₄H₅₄O₆
Molecular Weight:558.799
Hs Code.:

Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

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Chemical Property of Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

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Technology Process of Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

There total 4 articles about Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77012-06-7
Tetradecanoic acid (3S,3aR,6aS,7R,8S,10R,10aR,10bS)-3,3a,8,10a-tetrahydroxy-7-isopropenyl-2,10-dimethyl-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

: 77012-07-8
Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

Guidance literature:: With manganese(IV) oxide; In acetone; benzene; for 12h;
DOI:10.1515/znb-1980-1130

Reference yield:

: 18325-99-0
(3aR,6aS,7R,10R,10aR,10bS)-3a,10a-dihydroxy-5-(hydroxymethyl)-2,10-dimethyl-7-(prop-1-en-2-yl)-3a,4,6a,7,10,10a-hexahydrobenzo[e]azulene-3,8(9H,10bH)-dione

: 77012-07-8
Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: 19 percent / NaBH₄ / ethanol; H₂O / 3 h

3: MnO₂ / acetone; benzene / 12 h

With pyridine; manganese(IV) oxide; sodium tetrahydroborate; In ethanol; water; acetone; benzene;
DOI:10.1515/znb-1980-1130

Reference yield:

: 77012-05-6
Tetradecanoic acid (3aR,6aS,7R,10R,10aR,10bS)-3a,10a-dihydroxy-7-isopropenyl-2,10-dimethyl-3,8-dioxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

: 77012-07-8
Tetradecanoic acid (3aR,6aS,7R,8S,10R,10aR,10bS)-3a,8,10a-trihydroxy-7-isopropenyl-2,10-dimethyl-3-oxo-3,3a,4,6a,7,8,9,10,10a,10b-decahydro-benzo[e]azulen-5-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / NaBH₄ / ethanol; H₂O / 3 h

2: MnO₂ / acetone; benzene / 12 h

With manganese(IV) oxide; sodium tetrahydroborate; In ethanol; water; acetone; benzene;
DOI:10.1515/znb-1980-1130