(+/-)-Pulo'upone

Base Information

Chemical Name:(+/-)-Pulo'upone
CAS No.:119650-31-6
Molecular Formula:C₂₁H₂₇NO
Molecular Weight:309.451
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-Pulo'upone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-Pulo'upone

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (+/-)-Pulo'upone

There total 7 articles about (+/-)-Pulo'upone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153432-18-9
(2E,4E,8E)-10-Pyridin-2-yl-deca-2,4,8-trien-1-ol

: 97190-30-2,119650-31-6,120442-04-8,123807-89-6,123807-91-0
(+/-)-Pulo'upone

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / pyridine

2: 55 percent / dilithium tetrachlorocuprate / tetrahydrofuran / 3 h / -30 °C

3: 95 percent / 10percent H₂SO₄ / acetone

4: 70 percent / K₂CO₃ / dioxane; H₂O / 95 °C

5: toluene / 48 h / 110 °C / sealed ampoule

With pyridine; sulfuric acid; potassium carbonate; dilithium tetrachlorocuprate; In tetrahydrofuran; 1,4-dioxane; water; acetone; toluene;
DOI:10.1016/S0040-4020(01)88024-8

Reference yield:

: 153432-19-0
10-(2-pyridyl)-2E,4E,8E-decatrien-1-ol acetate

: 97190-30-2,119650-31-6,120442-04-8,123807-89-6,123807-91-0
(+/-)-Pulo'upone

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / dilithium tetrachlorocuprate / tetrahydrofuran / 3 h / -30 °C

2: 95 percent / 10percent H₂SO₄ / acetone

3: 70 percent / K₂CO₃ / dioxane; H₂O / 95 °C

4: toluene / 48 h / 110 °C / sealed ampoule

With sulfuric acid; potassium carbonate; dilithium tetrachlorocuprate; In tetrahydrofuran; 1,4-dioxane; water; acetone; toluene;
DOI:10.1016/S0040-4020(01)88024-8

Reference yield:

: 153432-16-7
ethyl 10-(2-pyridyl)-2E,4E,8E-decatrienoate

: 97190-30-2,119650-31-6,120442-04-8,123807-89-6,123807-91-0
(+/-)-Pulo'upone

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / LiAlH₄ / diethyl ether / 1 h / -30 °C

2: 95 percent / pyridine

3: 55 percent / dilithium tetrachlorocuprate / tetrahydrofuran / 3 h / -30 °C

4: 95 percent / 10percent H₂SO₄ / acetone

5: 70 percent / K₂CO₃ / dioxane; H₂O / 95 °C

6: toluene / 48 h / 110 °C / sealed ampoule

With pyridine; lithium aluminium tetrahydride; sulfuric acid; potassium carbonate; dilithium tetrachlorocuprate; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water; acetone; toluene;
DOI:10.1016/S0040-4020(01)88024-8