(+)-(3S,4S)-trans-3-bromo-4-menthyloxyacetoxy-1,2,3,4-tetrahydrobenzanthracene

Base Information

• Chemical Name: (+)-(3S,4S)-trans-3-bromo-4-menthyloxyacetoxy-1,2,3,4-tetrahydrobenz
• Molecular Formula: C₃₀H₃₅BrO₃
• Molecular Weight: 523.51

Synonyms:

Chemical Property of (+)-(3S,4S)-trans-3-bromo-4-menthyloxyacetoxy-1,2,3,4-tetrahydrobenz

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

There total 1 articles about (+)-(3S,4S)-trans-3-bromo-4-menthyloxyacetoxy-1,2,3,4-tetrahydrobenzanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-menthoxyacetyl chloride (15356-62-4) + (+/-)-trans-3-bromo-1,2,3,4-tetrahydrobenzanthracen-4-ol → (+)-(3S,4S)-trans-3-bromo-4-menthyloxyacetoxy-1,2,3,4-tetrahydrobenzanthracene (148260-34-8) + (-)-(3R,4R)-trans-3-bromo-4-menthyloxyacetoxy-1,2,3,4-tetrahydrobenzanthracene (148190-91-4)

Guidance literature:

With pyridine; Yield given. Yields of byproduct given;

Reference yield:

(+)-(3S,4S)-trans-3-bromo-4-menthyloxyacetoxy-1,2,3,4-tetrahydrobenzanthracene (148260-34-8) → (-)-(3R,4S)-3,4-epoxy-1,2,3,4-tetrahydrobenzanthracene (89618-18-8,89618-17-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / B₂H₆*THF / tetrahydrofuran / 144 h / Ambient temperature

2: basic form of Amberlite resin IRA-400 / tetrahydrofuran / 18 h / Ambient temperature

With B₂H₆-THF; basic form of Amberlite resin IRA-400; In tetrahydrofuran;

upstream raw materials:

L-menthoxyacetyl chloride

Downstream raw materials:

(-)-(3R,4S)-3,4-epoxy-1,2,3,4-tetrahydrobenzanthracene

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