5-tert-butyl-2-methyl-3-nitro-benzonitrile

Base Information

Chemical Name:5-tert-butyl-2-methyl-3-nitro-benzonitrile
CAS No.:858843-82-0
Molecular Formula:C₁₂H₁₄N₂O₂
Molecular Weight:218.255
Hs Code.:

5-<i>tert</i>-butyl-2-methyl-3-nitro-benzonitrile

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-tert-butyl-2-methyl-3-nitro-benzonitrile

Chemical Property:

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Technology Process of 5-tert-butyl-2-methyl-3-nitro-benzonitrile

There total 3 articles about 5-tert-butyl-2-methyl-3-nitro-benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 858843-55-7
5-(tert-butyl)-2-methyl-3-nitroaniline

: 858843-82-0
5-tert-butyl-2-methyl-3-nitro-benzonitrile

Guidance literature:: With sulfuric acid; Diazotization_.Eintragen der Diazoniumsalz-Loesung in eine aus Natriumcyanid, Kupfer(II)-sulfat und Wasser hergestellte Loesung und anschliessend Erwaermen;
DOI:10.1039/jr9340001954

Reference yield:

: 98-51-1
4-tert-butyltoluene

: 858843-82-0
5-tert-butyl-2-methyl-3-nitro-benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: fuming sulfuric acid; HNO₃

2: water; ethanol; ammonium sulfide

3: aqueous sulfuric acid / Diazotization_.Eintragen der Diazoniumsalz-Loesung in eine aus Natriumcyanid, Kupfer(II)-sulfat und Wasser hergestellte Loesung und anschliessend Erwaermen

With ammonium sulfide; ethanol; sulfuric acid; water; nitric acid;
DOI:10.1039/jr9340001954

Reference yield:

: 4162-89-4
4-(tert-butyl)-2,6-dinitrotoluene

: 858843-82-0
5-tert-butyl-2-methyl-3-nitro-benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: water; ethanol; ammonium sulfide

2: aqueous sulfuric acid / Diazotization_.Eintragen der Diazoniumsalz-Loesung in eine aus Natriumcyanid, Kupfer(II)-sulfat und Wasser hergestellte Loesung und anschliessend Erwaermen

With ammonium sulfide; ethanol; sulfuric acid; water;
DOI:10.1039/jr9340001954