C₁₅H₂₄O₂

Base Information

Chemical Name:C₁₅H₂₄O₂
CAS No.:1392491-89-2
Molecular Formula:C₁₅H₂₄O₂
Molecular Weight:236.354
Hs Code.:

C<sub>15</sub>H<sub>24</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₄O₂

Chemical Property:

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Technology Process of C₁₅H₂₄O₂

There total 11 articles about C₁₅H₂₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (-)-(3S,5R,6S,9S)-6-(2-hydroxypropan-2-yl)-3-isopropyl-9-methyl-1-oxaspiro[4.4]nonan-2-one

: 1392491-89-2
C₁₅H₂₄O₂

: 98263-92-4,101392-04-5,117141-65-8,146142-59-8,146142-60-1
(1S,4S,5R,7S)-curcumalactone

Guidance literature:: With thionyl chloride; In dichloromethane; at 23 ℃; for 40h; Inert atmosphere;
DOI:10.1021/ja303414a

Reference yield:

: 71037-85-9
4-(1-methyl-2,5-dioxocyclopentyl)butanoic acid

: 1392491-89-2
C₁₅H₂₄O₂

: 98263-92-4,101392-04-5,117141-65-8,146142-59-8,146142-60-1
(1S,4S,5R,7S)-curcumalactone

Guidance literature:: Multi-step reaction with 9 steps

1.1: 2-phenyl-3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; lithium chloride / dichloromethane / 25 h / Inert atmosphere

2.1: disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 120 h / 23 °C / Inert atmosphere

3.1: trimethylsilyl trifluoromethanesulfonate / benzene / 144 h / 0 - 23 °C / Inert atmosphere

4.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

4.2: 3 h / -78 - 0 °C / Inert atmosphere

4.3: 64 h / 0 - 23 °C / Inert atmosphere

5.1: triethylamine / 36 h / 50 °C / Inert atmosphere

6.1: Burgess Reagent / benzene / 8.5 h / Inert atmosphere; Reflux

6.2: 12 h / Inert atmosphere

7.1: cerium(III) chloride; lithium chloride / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

7.2: 0.5 h / -78 °C / Inert atmosphere

8.1: L-Selectride / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

9.1: thionyl chloride / dichloromethane / 40 h / 23 °C / Inert atmosphere

With disodium hydrogenphosphate; thionyl chloride; cerium(III) chloride; Burgess Reagent; trimethylsilyl trifluoromethanesulfonate; 2-phenyl-3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; L-Selectride; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; 3-chloro-benzenecarboperoxoic acid; lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ja303414a

Reference yield:

: 765-69-5
2-Methylcyclopentane-1,3-dione

: 1392491-89-2
C₁₅H₂₄O₂

: 98263-92-4,101392-04-5,117141-65-8,146142-59-8,146142-60-1
(1S,4S,5R,7S)-curcumalactone

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydroxide / water / 72 h / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 24 h

3.1: 2-phenyl-3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; lithium chloride / dichloromethane / 25 h / Inert atmosphere

4.1: disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 120 h / 23 °C / Inert atmosphere

5.1: trimethylsilyl trifluoromethanesulfonate / benzene / 144 h / 0 - 23 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

6.2: 3 h / -78 - 0 °C / Inert atmosphere

6.3: 64 h / 0 - 23 °C / Inert atmosphere

7.1: triethylamine / 36 h / 50 °C / Inert atmosphere

8.1: Burgess Reagent / benzene / 8.5 h / Inert atmosphere; Reflux

8.2: 12 h / Inert atmosphere

9.1: cerium(III) chloride; lithium chloride / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

10.1: L-Selectride / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

11.1: thionyl chloride / dichloromethane / 40 h / 23 °C / Inert atmosphere

With disodium hydrogenphosphate; thionyl chloride; cerium(III) chloride; Burgess Reagent; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; 2-phenyl-3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; hydrogen; tetra-(n-butyl)ammonium iodide; L-Selectride; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; 3-chloro-benzenecarboperoxoic acid; lithium chloride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; benzene;
DOI:10.1021/ja303414a