Technology Process of 4-methylicosane
There total 8 articles about 4-methylicosane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 47 mg / hydrogen / 5 percent Pd-CaCO3 / benzene / 760 Torr / Ambient temperature
2: 6 mg / hydrogen / 5 percent Pd-CaCO3 / benzene / 760 Torr / Ambient temperature
3: 150 mg / LiALH4 / tetrahydrofuran / 3 h / Ambient temperature
4: 1.) MeSO2Cl, pyridine; 2.) LiAlH4 / 1.) 36 h, room temperature; 2.) Et2O, 24 h, room temperature
With
pyridine; lithium aluminium tetrahydride; hydrogen; methanesulfonyl chloride;
Lindlar's catalyst;
In
tetrahydrofuran; benzene;
DOI:10.1016/S0031-9422(00)84166-7
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 6 mg / hydrogen / 5 percent Pd-CaCO3 / benzene / 760 Torr / Ambient temperature
2: 150 mg / LiALH4 / tetrahydrofuran / 3 h / Ambient temperature
3: 1.) MeSO2Cl, pyridine; 2.) LiAlH4 / 1.) 36 h, room temperature; 2.) Et2O, 24 h, room temperature
With
pyridine; lithium aluminium tetrahydride; hydrogen; methanesulfonyl chloride;
Lindlar's catalyst;
In
tetrahydrofuran; benzene;
DOI:10.1016/S0031-9422(00)84166-7
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 22 mg / hydrogen / 5 percent Pd-CaCO3 / benzene / 760 Torr / Ambient temperature
2: 150 mg / LiALH4 / tetrahydrofuran / 3 h / Ambient temperature
3: 1.) MeSO2Cl, pyridine; 2.) LiAlH4 / 1.) 36 h, room temperature; 2.) Et2O, 24 h, room temperature
With
pyridine; lithium aluminium tetrahydride; hydrogen; methanesulfonyl chloride;
Lindlar's catalyst;
In
tetrahydrofuran; benzene;
DOI:10.1016/S0031-9422(00)84166-7
