glycocholic acid 3-glucuronide disodium salt

Base Information

Chemical Name:glycocholic acid 3-glucuronide disodium salt
CAS No.:75672-42-3
Molecular Formula:C₃₂H₄₉NO₁₂*2Na
Molecular Weight:685.72
Hs Code.:

Synonyms:

Suppliers and Price of glycocholic acid 3-glucuronide disodium salt

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of glycocholic acid 3-glucuronide disodium salt

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

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Technology Process of glycocholic acid 3-glucuronide disodium salt

There total 5 articles about glycocholic acid 3-glucuronide disodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6919-98-8
2,3,4-tri-O-acetyl-1-bromo-1-deoxy-β-D-glucopyranuronic acid methy ester

: 75672-42-3
glycocholic acid 3-glucuronide disodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N,N'-dicyclohexylcarbodiimide / 2.) CdCO₃ / 1.) AcOEt, dioxane, room temp., 2.) toluene, reflux

2: pyridine / Ambient temperature

3: 20 mg / 7percent NaOH / methanol / 32 h / 40 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; cadmium(II) carbonate; In pyridine; methanol;
DOI:10.1248/cpb.28.1258

Reference yield:

: 75672-40-1
ethyl 7,12-diformylglycocholate 3-glucuronide acetate-methyl ester

: 75672-42-3
glycocholic acid 3-glucuronide disodium salt

Guidance literature:: With sodium hydroxide; In methanol; at 40 ℃; for 32h;
DOI:10.1248/cpb.28.1258

Reference yield:

: 64986-86-3
3α-hydroxy-7α,12α-diformyloxy-5β-cholan-24-oic acid

: 75672-42-3
glycocholic acid 3-glucuronide disodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N,N'-dicyclohexylcarbodiimide / 2.) CdCO₃ / 1.) AcOEt, dioxane, room temp., 2.) toluene, reflux

2: pyridine / Ambient temperature

3: 20 mg / 7percent NaOH / methanol / 32 h / 40 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; cadmium(II) carbonate; In pyridine; methanol;
DOI:10.1248/cpb.28.1258