tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate

Base Information

Chemical Name:tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate
CAS No.:1203486-73-0
Molecular Formula:C₁₅H₂₃N₃O₃
Molecular Weight:293.366
Hs Code.:

Synonyms:

Suppliers and Price of tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
(6-Morpholin-4-ylmethyl-pyridin-3-yl)-carbamic acid tert-butyl ester 95%+
1g
$ 1025.00

Matrix Scientific
(6-Morpholin-4-ylmethyl-pyridin-3-yl)-carbamic acid tert-butyl ester 95%+
500mg
$ 668.00

Advanced Chemicals Intermediatesced Chemicals Intermediates
(6-Morpholin-4-ylmethyl-pyridin-3-yl)-carbamicacidtert-butylester 95%+
5g
$ 1442.75

Acints
(6-Morpholin-4-ylmethyl-pyridin-3-yl)-carbamicacidtert-butylester 95%+
5g
$ 1442.75

Acints
(6-Morpholin-4-ylmethyl-pyridin-3-yl)-carbamicacidtert-butylester 95%+
1g
$ 500.25

Acints
(6-Morpholin-4-ylmethyl-pyridin-3-yl)-carbamicacidtert-butylester 95%+
500mg
$ 326.25

Total 3 raw suppliers

Chemical Property of tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

(6-Morpholin-4-ylmethyl-pyridin-3-yl)-carbamic acid tert-butyl ester 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate

There total 5 articles about tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 882424-73-9
(5-(tert-butoxycarbonylamino)pyridin-2-yl)methyl methanesulfonate

: 1203486-73-0
tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 12h;

Reference yield:

: 24242-20-4,114849-40-0
5-amino-pyridine-2-carboxylic acid

: 1203486-73-0
tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 12 h / Reflux

2.1: dmap / tert-butyl alcohol; acetone / 20 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 3.5 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 0 °C

4.2: 0 °C

5.1: potassium carbonate / acetonitrile / 12 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; dmap; In tetrahydrofuran; diethyl ether; acetone; acetonitrile; tert-butyl alcohol;

Reference yield:

: 119830-47-6
ethyl 3-amino-pyridine-6-carboxylate

: 1203486-73-0
tert-butyl 6-(morpholinomethyl)pyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap / tert-butyl alcohol; acetone / 20 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 3.5 h / 0 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 0 °C

3.2: 0 °C

4.1: potassium carbonate / acetonitrile / 12 h / 20 °C

With lithium aluminium tetrahydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; dmap; In tetrahydrofuran; diethyl ether; acetone; acetonitrile; tert-butyl alcohol;