N-hydroxy Rhodamine B amide

Base Information

• Chemical Name: N-hydroxy Rhodamine B amide
• CAS No.: 1115867-62-3
• Molecular Formula: C₂₈H₃₁N₃O₃
• Molecular Weight: 457.572
• Mol file: 1115867-62-3.mol

Synonyms:

Chemical Property of N-hydroxy Rhodamine B amide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-hydroxy Rhodamine B amide

There total 6 articles about N-hydroxy Rhodamine B amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

rhodamine B (509-34-2) → rhodamine hydroxamic acid (1115867-62-3)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; for 10h; Reflux;

DOI:10.1039/c7ob02858j

Reference yield: 89.0%

rhodamine B → rhodamine hydroxamic acid (1115867-62-3)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 80 ℃;

Reference yield: 80.0%

rhodamine B (81-88-9) → rhodamine hydroxamic acid (1115867-62-3)

Guidance literature:

With hydroxylamine; sodium hydroxide; In ethanol; at 20 ℃; for 2h;

DOI:10.1039/c0cc02881a

upstream raw materials:

N-(9-(2-(chlorocarbonyl)phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethylethanaminium

rhodamine B

rhodamine B

Refernces

• 1、 Yang, Young-Keun,Cho, Hyungseoph Jason,Lee, Jihyun,Shin, Injae,Tae, Jinsung. "A rhodamine-hydroxamic acid-based fluorescent probe for hypochlorous acid and its applications to Biological imagings". . p. 859 - 861. Retrieved 2009.
• 2、 Wu, Cong,Bian, Qing-Na,Zhang, Bian-Guo,Cai, Xin,Zhang, Shu-Dong,Zheng, Hong,Yang, Shi-Yao,Jiang, Yun-Bao. "Ring expansion of spiro-thiolactam in rhodamine scaffold: Switching the recognition preference by adding one atom". . p. 4198 - 4201. Retrieved 2012.
• 3、 Yoo, Jae Hoon,Lee, Yu Jeong,Lee, Kang Min,Choi, Myung Gil,Park, Tae Jung,Chang, Suk-Kyu. "Determination of thallium(iii) ions by oxidative hydrolysis of rhodamine-hydroxamate". . p. 603 - 609. Retrieved 2021.
• 4、 Kim, Hyemi,Moon, Kyung-Soo,Shim, Soyoung,Tae, Jinsung. "Cyclen-conjugated rhodamine hydroxamate as Pd2+-specific fluorescent chemosensor". . p. 1987 - 1991. Retrieved 2011.
• 5、 -. "Fluorescent probe for detecting hypochlorous acid, and synthesis method and application thereof". Paragraph 0017. . Retrieved 2019/02/13.
• 6、 Nakamura, Akira,Kanou, Hodaka,Tanaka, Junki,Imamiya, Akira,Maegawa, Tomohiro,Miki, Yasuyoshi. "A mild method for synthesizing carboxylic acids by oxidation of aldoximes using hypervalent iodine reagents". supporting information. p. 541 - 544. Retrieved 2018/02/07.