C₂₂H₁₈ClNO₃

Base Information

Chemical Name:C₂₂H₁₈ClNO₃
CAS No.:1448892-39-4
Molecular Formula:C₂₂H₁₈ClNO₃
Molecular Weight:379.843
Hs Code.:

C<sub>22</sub>H<sub>18</sub>ClNO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₈ClNO₃

Chemical Property:

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Technology Process of C₂₂H₁₈ClNO₃

There total 9 articles about C₂₂H₁₈ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1448892-46-3
C₂₂H₁₉NO₄

: 1448892-39-4
C₂₂H₁₈ClNO₃

Guidance literature:: With tetrachloromethane; triphenylphosphine; In 1,2-dichloro-ethane; at 50 ℃; for 18h; Inert atmosphere;
DOI:10.3987/COM-12-S(N)37

Reference yield:

: 92-70-6
3-Hydroxy-2-naphthoic acid

: 1448892-39-4
C₂₂H₁₈ClNO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: ammonium hydroxide; zinc(II) chloride / water / 108 h / 190 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / n-heptan1ol / 19 h / Inert atmosphere; Reflux

3.1: zinc(II) chloride; N-Bromosuccinimide / acetone / 2 h / -78 °C / Inert atmosphere

4.1: potassium carbonate; copper(l) chloride / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

5.1: palladium on activated charcoal; hydrogen; quinoline / acetone / 2.5 h / 20 °C / 760.05 Torr / Inert atmosphere

6.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide; 1,4-diaza-bicyclo[2.2.2]octane / water; acetone / 72 h / 0 °C / Inert atmosphere

7.1: pyridine / 0.5 h / 0 °C / Inert atmosphere

7.2: 1 h

7.3: 3 h / 20 °C

8.1: n-butyllithium / tetrahydrofuran; hexane / 20 h / -78 - 20 °C / Inert atmosphere

9.1: triphenylphosphine; tetrachloromethane / 1,2-dichloro-ethane / 18 h / 50 °C / Inert atmosphere

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; quinoline; tetrachloromethane; potassium osmate(VI) dihydrate; ammonium hydroxide; N-Bromosuccinimide; n-butyllithium; palladium on activated charcoal; hydrogen; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triphenylphosphine; copper(l) chloride; zinc(II) chloride; In tetrahydrofuran; hexane; n-heptan1ol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.3987/COM-12-S(N)37

Reference yield:

: 5959-52-4
2-Amino-3-naphthoic acid

: 1448892-39-4
C₂₂H₁₈ClNO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene-4-sulfonic acid / n-heptan1ol / 19 h / Inert atmosphere; Reflux

2.1: zinc(II) chloride; N-Bromosuccinimide / acetone / 2 h / -78 °C / Inert atmosphere

3.1: potassium carbonate; copper(l) chloride / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

4.1: palladium on activated charcoal; hydrogen; quinoline / acetone / 2.5 h / 20 °C / 760.05 Torr / Inert atmosphere

5.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide; 1,4-diaza-bicyclo[2.2.2]octane / water; acetone / 72 h / 0 °C / Inert atmosphere

6.1: pyridine / 0.5 h / 0 °C / Inert atmosphere

6.2: 1 h

6.3: 3 h / 20 °C

7.1: n-butyllithium / tetrahydrofuran; hexane / 20 h / -78 - 20 °C / Inert atmosphere

8.1: triphenylphosphine; tetrachloromethane / 1,2-dichloro-ethane / 18 h / 50 °C / Inert atmosphere

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; quinoline; tetrachloromethane; potassium osmate(VI) dihydrate; N-Bromosuccinimide; n-butyllithium; palladium on activated charcoal; hydrogen; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triphenylphosphine; copper(l) chloride; zinc(II) chloride; In tetrahydrofuran; hexane; n-heptan1ol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.3987/COM-12-S(N)37