methyl(2-furyl)zirconocene

Base Information

• Chemical Name: methyl(2-furyl)zirconocene
• CAS No.: 139167-68-3
• Molecular Formula: C₁₅H₁₆OZr
• Molecular Weight: 303.515

Synonyms:

Chemical Property of methyl(2-furyl)zirconocene

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Technology Process of methyl(2-furyl)zirconocene

There total 1 articles about methyl(2-furyl)zirconocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-lithiofuran (2786-02-9) + zirconocene methyl chloride → bis(cyclopentadienyl)dimethylzirconium(IV) (12636-72-5) + bis(2-furyl)zirconocen + methyl(2-furyl)zirconocene (139167-68-3)

Guidance literature:

In diethyl ether; byproducts: LiCl; inert atm., Schlenk technique; soln. of Zr-complex in ether cooled (-78°C), dropwise addn. of Li-salt in ether, warmed (over 12 h to ambient temp. with stirring); evapn., extn. (CHCl3), filtration, evapn. (brownish solid), mixt. not further purified; elem. anal., IR;;

DOI:10.1021/om00040a040

upstream raw materials:

2-lithiofuran

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