methyltriphenylphosphonium methylcarbonate

Base Information

• Chemical Name: methyltriphenylphosphonium methylcarbonate
• CAS No.: 1067966-63-5
• Molecular Formula: C₂H₃O₃*C₁₉H₁₈P
• Molecular Weight: 352.37
• Mol file: 1067966-63-5.mol

Synonyms:

Chemical Property of methyltriphenylphosphonium methylcarbonate

Chemical Property:

• Melting Point: 146-151°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

Methyltriphenylphosphonium methylcarbonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Methyltriphenylphosphonium Methylcarbonate is a wittig vinylation reagent.

Technology Process of methyltriphenylphosphonium methylcarbonate

There total 1 articles about methyltriphenylphosphonium methylcarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

triphenylphosphine (603-35-0) + carbonic acid dimethyl ester (616-38-6) → methyltriphenylphosphonium methylcarbonate (1067966-63-5)

Guidance literature:

In methanol; at 140 ℃; for 24h; Inert atmosphere;

DOI:10.1002/cssc.201500935

upstream raw materials:

triphenylphosphine

carbonic acid dimethyl ester

Refernces

• 1、 Cattelan, Lisa,Noè, Marco,Selva, Maurizio,Demitri, Nicola,Perosa, Alvise. "Methyltriphenylphosphonium Methylcarbonate, an All-In-One Wittig Vinylation Reagent". . p. 3963 - 3966. Retrieved 2015/12/17.