5-Phenyl-1-(p-tolyl)-1H-pyrazole

Base Information

Chemical Name:5-Phenyl-1-(p-tolyl)-1H-pyrazole
CAS No.:943725-79-9
Molecular Formula:C₁₆H₁₄N₂
Molecular Weight:234.301
Hs Code.:
DSSTox Substance ID:DTXSID60589427
Nikkaji Number:J3.556.177C
Wikidata:Q82482786
Mol file:943725-79-9.mol

Synonyms:5-Phenyl-1-(p-tolyl)-1H-pyrazole;943725-79-9;1-(4-Methylphenyl)-5-phenyl-1H-pyrazole;SCHEMBL12759885;DTXSID60589427;AKOS010626768;A12156

Suppliers and Price of 5-Phenyl-1-(p-tolyl)-1H-pyrazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
5-Phenyl-1-(p-tolyl)-1H-pyrazole 95+%
1g
$ 313.00

Alichem
5-Phenyl-1-(p-tolyl)-1H-pyrazole
1g
$ 400.00

Total 3 raw suppliers

Chemical Property of 5-Phenyl-1-(p-tolyl)-1H-pyrazole

Chemical Property:

Boiling Point:387.3±21.0 °C(Predicted)
PKA:0.11±0.10(Predicted)
Density:1.06±0.1 g/cm3(Predicted)
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:234.115698455
Heavy Atom Count:18
Complexity:252

Purity/Quality:

97% ^*data from raw suppliers

5-Phenyl-1-(p-tolyl)-1H-pyrazole 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N2C(=CC=N2)C3=CC=CC=C3

Technology Process of 5-Phenyl-1-(p-tolyl)-1H-pyrazole

There total 4 articles about 5-Phenyl-1-(p-tolyl)-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88254-47-1
(E)-1-(4-tolyl)-2-((E)-3-phenylallylidene)hydrazone

: 91-22-5
quinoline

: 20518-17-6
1-(4-methylphenyl)-1H-pyrazole

: 106-49-0,12221-03-3
p-toluidine

: 943725-79-9
5-phenyl-1-(p-tolyl)-1H-pyrazole

Guidance literature:: at 600 ℃; for 0.666667h; under 0.001 - 0.005 Torr; Further byproducts given. Title compound not separated from byproducts;

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 943725-79-9
5-phenyl-1-(p-tolyl)-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetraisopropoxide / tetrahydrofuran / 0 - 20 °C

2: copper diacetate / acetonitrile / 0.08 h / 20 °C / Schlenk technique; Inert atmosphere

With titanium tetraisopropoxide; copper diacetate; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c9cc09657d

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 943725-79-9
5-phenyl-1-(p-tolyl)-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: tetrafluoroboric acid; tert.-butylnitrite / ethanol; water / 1 h / 0 - 20 °C

2: copper diacetate / acetonitrile / 0.08 h / 20 °C / Schlenk technique; Inert atmosphere

With tetrafluoroboric acid; tert.-butylnitrite; copper diacetate; In ethanol; water; acetonitrile;
DOI:10.1039/c9cc09657d