rac N-Boc-anatabine

Base Information

Chemical Name:rac N-Boc-anatabine
CAS No.:1159977-12-4
Molecular Formula:C₁₅H₂₀N₂O₂
Molecular Weight:260.336
Hs Code.:
Mol file:1159977-12-4.mol

Synonyms:

Suppliers and Price of rac N-Boc-anatabine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
rac-N-boc anatabine
5mg
$ 440.00

TRC
rac-N-BocAnatabine
100mg
$ 1230.00

Total 2 raw suppliers

Chemical Property of rac N-Boc-anatabine

Chemical Property:

Boiling Point:364.5±42.0 °C(Predicted)
PKA:5.06±0.12(Predicted)
Density:1.105±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

rac-N-boc anatabine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Anatabine (A637500) derivative.

Technology Process of rac N-Boc-anatabine

There total 5 articles about rac N-Boc-anatabine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: tert-butyl allyl[1-(pyridin-3-yl)but-3-en-1-yl]carbamate

: 1159977-12-4
tert-butyl 3,6-dihydro-[2,3'-bipyridine]-1(2H)-carboxylate

Guidance literature:: tert-butyl allyl[1-(pyridin-3-yl)but-3-en-1-yl]carbamate; With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 1h;

With Grubbs catalyst first generation; In dichloromethane; at 20 ℃; for 3h; Reagent/catalyst; Solvent;
DOI:10.1055/s-0036-1591538

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 2743-90-0,126454-22-6
(+/-)-Anatabine

: 1159977-12-4
tert-butyl 3,6-dihydro-[2,3'-bipyridine]-1(2H)-carboxylate

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; for 8h; Cooling with ice; Inert atmosphere;

Reference yield:

: 500-22-1
3-pyridinecarboxaldehyde

: 1159977-12-4
tert-butyl 3,6-dihydro-[2,3'-bipyridine]-1(2H)-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2-methyltetrahydrofuran / 3 h / 20 °C / Molecular sieve

2.1: indium / ethanol / 4 h / 0 - 20 °C

3.1: potassium carbonate / 2-methyltetrahydrofuran / 24 h / 50 °C

4.1: toluene-4-sulfonic acid / dichloromethane / 1 h / 20 °C

4.2: 3 h / 20 °C

With indium; potassium carbonate; toluene-4-sulfonic acid; In 2-methyltetrahydrofuran; ethanol; dichloromethane;
DOI:10.1055/s-0036-1591538