2-indol-3-ylethyl toluene-p-sulphonate

Base Information

• Chemical Name: 2-indol-3-ylethyl toluene-p-sulphonate
• CAS No.: 6243-54-5
• Molecular Formula: C₁₇H₁₇NO₃S
• Molecular Weight: 315.393

Synonyms:

Chemical Property of 2-indol-3-ylethyl toluene-p-sulphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-indol-3-ylethyl toluene-p-sulphonate

There total 1 articles about 2-indol-3-ylethyl toluene-p-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-indol-3-ylethyl toluene-p-sulphonate (6243-54-5)

Guidance literature:

aus Tryptophol;

Reference yield:

2-indol-3-ylethyl toluene-p-sulphonate (6243-54-5) → (-)-strempeliopine (79808-95-0)

Guidance literature:

Multi-step reaction with 6 steps

1.1: sodium hydride / toluene / 85 °C

1.2: 20 °C

2.1: trichlorophosphate / acetonitrile / 20 °C

3.1: sodium cyanoborohydride / ethanol / 20 °C

4.1: ozone / dichloromethane / -78 °C

5.1: 1,2-Diiodoethane; N,N,N,N,N,N-hexamethylphosphoric triamide; phenol; samarium / tetrahydrofuran / 20 °C

6.1: sodium hydride; carbon disulfide; methyl iodide; 1H-imidazole / tetrahydrofuran / 0 - 20 °C

6.2: 80 °C

With 1H-imidazole; carbon disulfide; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium; 1,2-Diiodoethane; sodium hydride; sodium cyanoborohydride; ozone; trichlorophosphate; methyl iodide; phenol; In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile; 6.1: |Barton-McCombie Deoxygenation / 6.2: |Barton-McCombie Deoxygenation;

DOI:10.1039/d1cc06278f

Downstream raw materials:

(-)-strempeliopine

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