22,22,22-d₃-docosanoic acid

Base Information

Chemical Name:22,22,22-d₃-docosanoic acid
CAS No.:1193721-67-3
Molecular Formula:C₂₂H₄₄O₂
Molecular Weight:343.566
Hs Code.:

Synonyms:

Suppliers and Price of 22,22,22-d₃-docosanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Medical Isotopes, Inc.
Docosanoic-22,22,22-d3Acid
100 mg
$ 690.00

American Custom Chemicals Corporation
DOCOSANOIC-22,22,22-D3 ACID 95.00%
5MG
$ 505.90

Total 2 raw suppliers

Chemical Property of 22,22,22-d₃-docosanoic acid

Chemical Property:

Melting Point:79 - 81°C

Purity/Quality:

97% ^*data from raw suppliers

Docosanoic-22,22,22-d3Acid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Docosanoic-22,22,22-d3 Acid can be used to study the neutron diffraction study on basic nanostructure of stratum corneum lipid matrices based on ceramides [EOS] and [AP]

Technology Process of 22,22,22-d₃-docosanoic acid

There total 17 articles about 22,22,22-d₃-docosanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 22,22,22-d₃-docosan-1-ol

: 1193721-67-3
22,22,22-d₃-docosanoic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In chloroform; acetone; at 0 ℃; for 3h;
DOI:10.1002/jlcr.3443

Reference yield:

: 29823-26-5,71607-34-6,1193721-67-3,1219804-98-4
Deuterisierte Docosansaeure

Guidance literature:: Docosansaeure, D2O;

Reference yield:

: 75949-34-7
methyl 9-[(tetrahydro-2H-pyran-2-yl)oxy]nonanoate

: 1193721-67-3
22,22,22-d₃-docosanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / diethyl ether / Reflux

2.1: triethylamine / chloroform / 14 h / 0 - 20 °C

3.1: lithium aluminium deuteride / diethyl ether / Heating

4.1: triphenylphosphine; bromine / dichloromethane / 12 h

5.1: magnesium / tetrahydrofuran / 3 h / 50 °C / Inert atmosphere

5.2: 3 h / -10 - -5 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / methanol / 3 h / Reflux

7.1: sulfuric acid; chromium(VI) oxide / chloroform; acetone / 3 h / 0 °C

With chromium(VI) oxide; lithium aluminium tetrahydride; lithium aluminium deuteride; sulfuric acid; bromine; pyridinium p-toluenesulfonate; magnesium; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; acetone; 5.1: |Grignard Reaction / 5.2: |Grignard Reaction;
DOI:10.1002/jlcr.3443