Ammonium methyl 2-O-sulfo-α-D-glucopyranoside

Base Information

Chemical Name:Ammonium methyl 2-O-sulfo-α-D-glucopyranoside
CAS No.:129189-45-3
Molecular Formula:C₇H₁₄O₉S*H₃N
Molecular Weight:291.279
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ammonium methyl 2-O-sulfo-α-D-glucopyranoside

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Technology Process of Ammonium methyl 2-O-sulfo-α-D-glucopyranoside

There total 2 articles about Ammonium methyl 2-O-sulfo-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 129261-64-9
methyl 3-O-nitro-2-O-sulfo-α-D-glucopyranoside

: 129189-45-3
Ammonium methyl 2-O-sulfo-α-D-glucopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In water; for 3h;
DOI:10.1016/0008-6215(90)84283-Z

Reference yield:

: 5115-94-6,13225-05-3
methyl 4,6-O-benzylidene-3-O-nitro-α-D-glucopyranoside

: 129189-45-3
Ammonium methyl 2-O-sulfo-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) SO₃-pyridine, 2) Dowex 50(H+) / 1) pyridine, a) 55 deg C, 4h, b) 25 deg C, 15h, 2) H₂O

2: 94 percent / H₂ / Pd/C / H₂O / 3 h

With pyridine-SO₃ complex; Dowex 50(H+); hydrogen; palladium on activated charcoal; In water;
DOI:10.1016/0008-6215(90)84283-Z