[2’,2’,3,3-²H₄]spirooxirane-2,3’-quinuclidine

Base Information

Chemical Name:[2’,2’,3,3-²H₄]spirooxirane-2,3’-quinuclidine
CAS No.:1627167-04-7
Molecular Formula:C₈H₁₃NO
Molecular Weight:143.166
Hs Code.:

[2’,2’,3,3-<sup>2</sup>H<sub>4</sub>]spirooxirane-2,3’-quinuclidine

Synonyms:

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Chemical Property of [2’,2’,3,3-²H₄]spirooxirane-2,3’-quinuclidine

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Technology Process of [2’,2’,3,3-²H₄]spirooxirane-2,3’-quinuclidine

There total 2 articles about [2’,2’,3,3-²H₄]spirooxirane-2,3’-quinuclidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 34291-53-7
[2,2-²H₂]-3-quinuclidinone

: 23726-00-3
<²H9>trimethylsulphoxonium iodide

: 1627167-04-7
[2’,2’,3,3-²H₄]spirooxirane-2,3’-quinuclidine

Guidance literature:: <²H9>trimethylsulphoxonium iodide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 5h;

[2,2-²H₂]-3-quinuclidinone; In N,N-dimethyl-formamide; mineral oil; for 0.5h;
DOI:10.1002/jlcr.3186

Reference yield:

: 3731-38-2
3-Quinuclidinone

: 1627167-04-7
[2’,2’,3,3-²H₄]spirooxirane-2,3’-quinuclidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium; deuteromethanol / Inert atmosphere; Reflux

1.2: 2.5 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 5 h

2.2: 0.5 h

With deuteromethanol; sodium; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/jlcr.3186