Ethyl alpha-cyano-2,3-dimethoxycinnamate

Base Information

Chemical Name:Ethyl alpha-cyano-2,3-dimethoxycinnamate
CAS No.:58531-09-2
Molecular Formula:C₁₄H₁₅NO₄
Molecular Weight:261.277
Hs Code.:
European Community (EC) Number:652-105-1

Synonyms:ETHYL ALPHA-CYANO-2,3-DIMETHOXYCINNAMATE;AKOS024333694;alpha-cyano-2,3-dimethoxycinnamic ethyl ester

Suppliers and Price of Ethyl alpha-cyano-2,3-dimethoxycinnamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl alpha-cyano-2,3-dimethoxycinnamate

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:261.10010796
Heavy Atom Count:19
Complexity:382

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C(=CC1=C(C(=CC=C1)OC)OC)C#N

Technology Process of Ethyl alpha-cyano-2,3-dimethoxycinnamate

There total 1 articles about Ethyl alpha-cyano-2,3-dimethoxycinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58531-09-2
ethyl 2-cyano-3-(2,3-dimethoxyphenyl)propenoate

Guidance literature:: /BRN= 908264/, Cyanessigsaeure-ethylester, Benzol, Eg., Zusatz von 6-Amino-hexansaeure;
DOI:10.1021/je60019a037

Reference yield: 22.0%

: 58531-09-2
ethyl 2-cyano-3-(2,3-dimethoxyphenyl)propenoate

: 128720-10-5
(E)-ethyl 2-cyano-3-(2-hydroxy-3-methoxyphenyl)propenoate

Guidance literature:: With sulfuric acid; Ambient temperature;

Reference yield:

: 58531-09-2
ethyl 2-cyano-3-(2,3-dimethoxyphenyl)propenoate

: 1729-02-8
3-ethoxycarbonyl-8-methoxycoumarin

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / H₂SO₄ / Ambient temperature

2: 67 percent / 10percent aq. HCl / ethanol / 0.5 h / Heating

With hydrogenchloride; sulfuric acid; In ethanol;