C₂₆H₃₉NO₄

Base Information

Chemical Name:C₂₆H₃₉NO₄
CAS No.:135615-62-2
Molecular Formula:C₂₆H₃₉NO₄
Molecular Weight:429.6
Hs Code.:

C<sub>26</sub>H<sub>39</sub>NO<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₆H₃₉NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₉NO₄

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₆H₃₉NO₄

There total 12 articles about C₂₆H₃₉NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133372-88-0
C₂₆H₃₄O₄

: 135615-62-2
C₂₆H₃₉NO₄

Guidance literature:: Multi-step reaction with 12 steps

1: KH / 5 h / 150 - 160 °C

2: thionyl chloride

4: thionyl chloride / benzene / 1.5 h

5: 1.) n-butyllithium / 1.) ether, hexane, 0 deg C, 80 min, 2.) -45 deg C, 0.25 h, then r.t., 0.75 h

6: 1.) ether, hexane, 0 deg C, 80 min, then r.t., 40 min, 2.) ether, r.t., 1 h

7: 127.5 mg / HBr / CH₂Cl₂ / 1.25 h / 0 °C

8: hydrogen / 10 percent Pd on charcoal / ethanol / 2.25 h / Ambient temperature

9: N-ethyldiisopropylamine / dimethylformamide / 1 h / Ambient temperature

10: lithium diisopropylamide / diethyl ether / 0.75 h / Ambient temperature

11: 1.) hydrogen, 2.) pyridine / 1.) 5 percent Rh on alumina / 1.) THF, 2.5 h, 2.) r.t., overnight

12: aq. acetic acid / tetrahydrofuran / 3 h / 50 °C

With pyridine; n-butyllithium; thionyl chloride; hydrogen bromide; hydrogen; potassium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium on activated charcoal; rhodium on alumina; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00019a051

Reference yield:

: 135615-59-7
C₂₅H₃₂O₄

: 135615-62-2
C₂₆H₃₉NO₄

Guidance literature:: Multi-step reaction with 11 steps

1: thionyl chloride

3: thionyl chloride / benzene / 1.5 h

4: 1.) n-butyllithium / 1.) ether, hexane, 0 deg C, 80 min, 2.) -45 deg C, 0.25 h, then r.t., 0.75 h

5: 1.) ether, hexane, 0 deg C, 80 min, then r.t., 40 min, 2.) ether, r.t., 1 h

6: 127.5 mg / HBr / CH₂Cl₂ / 1.25 h / 0 °C

7: hydrogen / 10 percent Pd on charcoal / ethanol / 2.25 h / Ambient temperature

8: N-ethyldiisopropylamine / dimethylformamide / 1 h / Ambient temperature

9: lithium diisopropylamide / diethyl ether / 0.75 h / Ambient temperature

10: 1.) hydrogen, 2.) pyridine / 1.) 5 percent Rh on alumina / 1.) THF, 2.5 h, 2.) r.t., overnight

11: aq. acetic acid / tetrahydrofuran / 3 h / 50 °C

With pyridine; n-butyllithium; thionyl chloride; hydrogen bromide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium on activated charcoal; rhodium on alumina; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00019a051

Reference yield:

: C₂₅H₃₁ClO₃

: 135615-62-2
C₂₆H₃₉NO₄

Guidance literature:: Multi-step reaction with 10 steps

2: thionyl chloride / benzene / 1.5 h

3: 1.) n-butyllithium / 1.) ether, hexane, 0 deg C, 80 min, 2.) -45 deg C, 0.25 h, then r.t., 0.75 h

4: 1.) ether, hexane, 0 deg C, 80 min, then r.t., 40 min, 2.) ether, r.t., 1 h

5: 127.5 mg / HBr / CH₂Cl₂ / 1.25 h / 0 °C

6: hydrogen / 10 percent Pd on charcoal / ethanol / 2.25 h / Ambient temperature

7: N-ethyldiisopropylamine / dimethylformamide / 1 h / Ambient temperature

8: lithium diisopropylamide / diethyl ether / 0.75 h / Ambient temperature

9: 1.) hydrogen, 2.) pyridine / 1.) 5 percent Rh on alumina / 1.) THF, 2.5 h, 2.) r.t., overnight

10: aq. acetic acid / tetrahydrofuran / 3 h / 50 °C

With pyridine; n-butyllithium; thionyl chloride; hydrogen bromide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium on activated charcoal; rhodium on alumina; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00019a051