[TiCl2(η5-C5Me5)(η5-C5Me4(CH2CH2CHCH)]

Base Information

Chemical Name:[TiCl2(η5-C5Me5)(η5-C5Me4(CH2CH2CHCH)]
CAS No.:547751-72-4
Molecular Formula:C₂₃H₃₄Cl₂Ti
Molecular Weight:429.309
Hs Code.:

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Chemical Property of [TiCl2(η5-C5Me5)(η5-C5Me4(CH2CH2CHCH)]

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Technology Process of [TiCl2(η5-C5Me5)(η5-C5Me4(CH2CH2CHCH)]

There total 1 articles about [TiCl2(η5-C5Me5)(η5-C5Me4(CH2CH2CHCH)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31168-87-3,18039-90-2
titanium trichloride tris(tetrahydrofuran)

: {1-(but-3-enyl)-2,3,4,5-tetramethylcyclopentadienyl}lithium

: lithiumpentamethylcyclopentadiene

: 11136-36-0
bis(pentamethylcyclopentadienyl)titanium dichloride

: 547751-72-4
[TiCl2(η5-C5Me5)(η5-C5Me4(CH2CH2CHCH)]

Guidance literature:: With PbCl₂; In tetrahydrofuran; diethyl ether; Ti-complex was mixed with Li-salt in THF, refluxed for 1 h, other Li-salt in Et2O was added, Et2O was distilled off, refluxed for 24 h, vol. wasreduced, PbCl2 was added under Ar, stirred for 2 h at 40°C under Ar; volatiles were evapd. under vac., extd. with hexane, crystd. from hexane;
DOI:10.1016/S0022-328X(02)02162-9