adenosylsuccinic acid ammonium salt

Base Information

Chemical Name:adenosylsuccinic acid ammonium salt
CAS No.:98675-17-3
Molecular Formula:C₁₄H₁₈N₅O₁₁P*H₃N
Molecular Weight:480.328
Hs Code.:

Synonyms:

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Chemical Property of adenosylsuccinic acid ammonium salt

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Technology Process of adenosylsuccinic acid ammonium salt

There total 11 articles about adenosylsuccinic acid ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5987-73-5
2',3',5'-O-triacetyl-6-chloroinosine

: 98675-17-3,139508-71-7
adenosylsuccinic acid ammonium salt

Guidance literature:: Multi-step reaction with 8 steps

1: 87 percent / triethylamine / methanol / 0.5 h / Ambient temperature

2: 97 percent / ammonia / methanol / Ambient temperature

3: 84 percent / toluene-4-sulphonic acid monohydrate / tetrahydrofuran / 1 h / 50 °C

4: 88 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 2.5 h / -5 °C

5: 70 percent / N,N-di-isopropylethylamine / N,N-dimethyl-acetamide / 28 h / 70 - 75 °C

6: 1.03 g / pyridine / 2 h / -40 °C

7: 0.734 g / aq. formic acid / 3 h / Ambient temperature

8: 1) hydrogen, 2) conc. aq. ammonia / 1) palladium on carbon / 1) RT, 1 atm, 2 h

With pyridine; ammonium hydroxide; formic acid; ammonia; hydrogen; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl acetamide;

Reference yield:

: 132089-81-7
6-(4-chlorophenylthio)-9-β-D-ribofuranosyl-9H-purine

: 98675-17-3,139508-71-7
adenosylsuccinic acid ammonium salt

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / toluene-4-sulphonic acid monohydrate / tetrahydrofuran / 1 h / 50 °C

2: 88 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 2.5 h / -5 °C

3: 70 percent / N,N-di-isopropylethylamine / N,N-dimethyl-acetamide / 28 h / 70 - 75 °C

4: 1.03 g / pyridine / 2 h / -40 °C

5: 0.734 g / aq. formic acid / 3 h / Ambient temperature

6: 1) hydrogen, 2) conc. aq. ammonia / 1) palladium on carbon / 1) RT, 1 atm, 2 h

With pyridine; ammonium hydroxide; formic acid; hydrogen; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide;

Reference yield:

: 132089-82-8
6-(4-chlorophenylthio)-9-(2,3-O-cyclopentylidene-β-D-ribofuranosyl)-9H-purine

: 98675-17-3,139508-71-7
adenosylsuccinic acid ammonium salt

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 2.5 h / -5 °C

2: 70 percent / N,N-di-isopropylethylamine / N,N-dimethyl-acetamide / 28 h / 70 - 75 °C

3: 1.03 g / pyridine / 2 h / -40 °C

4: 0.734 g / aq. formic acid / 3 h / Ambient temperature

5: 1) hydrogen, 2) conc. aq. ammonia / 1) palladium on carbon / 1) RT, 1 atm, 2 h

With pyridine; ammonium hydroxide; formic acid; hydrogen; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane; N,N-dimethyl acetamide;