Technology Process of C15H18O3
There total 3 articles about C15H18O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
Yield given;
1.) 0 deg C, 5 min, 2.) RT, 1 h;
DOI:10.1021/jo00379a001
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) lithium diisopropylamide, 2.) hexamethylphosphoric triamide (HMPA) / 1.) THF, -78 deg C, 20 min, 2.) THF, a) -78 deg C, 20 min, b) from -78 deg C to 0 deg C, 10 min
2: 40.0 mg / glacial acetic acid, 30percent H2O2 / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) RT, 30 min
3: pyridinium chlorochromate / CH2Cl2 / 1.) 0 deg C, 5 min, 2.) RT, 1 h
With
N,N,N,N,N,N-hexamethylphosphoric triamide; dihydrogen peroxide; acetic acid; pyridinium chlorochromate; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00379a001
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 40.0 mg / glacial acetic acid, 30percent H2O2 / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) RT, 30 min
2: pyridinium chlorochromate / CH2Cl2 / 1.) 0 deg C, 5 min, 2.) RT, 1 h
With
dihydrogen peroxide; acetic acid; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00379a001