Carbamic acid, (4-chlorophenyl)methyl-, methyl ester

Base Information

Chemical Name:Carbamic acid, (4-chlorophenyl)methyl-, methyl ester
CAS No.:60561-39-9
Molecular Formula:C9H10 Cl N O2
Molecular Weight:199.637
Hs Code.:
DSSTox Substance ID:DTXSID10209365
Wikidata:Q83083636

Synonyms:Carbamic acid, (4-chlorophenyl)methyl-, methyl ester;60561-39-9;N-(p-Chlorophenyl)-N-methyl-O-methyl carbamate;DTXSID10209365

Suppliers and Price of Carbamic acid, (4-chlorophenyl)methyl-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Carbamic acid, (4-chlorophenyl)methyl-, methyl ester

Chemical Property:

Vapor Pressure:0.00408mmHg at 25°C
Boiling Point:279.2°C at 760 mmHg
Flash Point:122.6°C
Density:1.252g/cm³
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:199.0400063
Heavy Atom Count:13
Complexity:179

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=C(C=C1)Cl)C(=O)OC

Technology Process of Carbamic acid, (4-chlorophenyl)methyl-, methyl ester

There total 3 articles about Carbamic acid, (4-chlorophenyl)methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-47-8
4-chloro-aniline

: 616-38-6
carbonic acid dimethyl ester

: 932-96-7
N-methyl(p-chloroaniline)

: 60561-39-9
p-Chlorphenyl-N-methyl-carbamidsaeure-methylester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1-methyl-pyrrolidin-2-one; at 200 ℃; for 0.2h; Reagent/catalyst; Temperature; Flow reactor;
DOI:10.1016/j.tet.2017.11.068

Reference yield:

: 106-47-8
4-chloro-aniline

: 60561-39-9
p-Chlorphenyl-N-methyl-carbamidsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / 1,2-dichloro-ethane; water / 3 h / 40 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene

With sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2017.11.068