N-ε-azido-L-lysine hydrochloride

Base Information

• Chemical Name: N-ε-azido-L-lysine hydrochloride
• CAS No.: 1454334-76-9
• Molecular Formula: C₆H₁₂N₄O₂*ClH
• Molecular Weight: 208.648

Synonyms:

Chemical Property of N-ε-azido-L-lysine hydrochloride

Chemical Property:

Purity/Quality:

98-101% (Assay by titration) ^*data from raw suppliers

L-Azidonorleucinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-ε-azido-L-lysine hydrochloride

There total 2 articles about N-ε-azido-L-lysine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dicyclohexylammonium N-tert-butyloxycarbonyl-2-amino-6-azidohexanoate (846549-33-5) → N-ε-azido-L-lysine hydrochloride (1454334-76-9)

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃; for 4h;

DOI:10.1039/c4cc03721a

Reference yield:

Boc-Lys-OH (13734-28-6) → N-ε-azido-L-lysine hydrochloride (1454334-76-9)

Guidance literature:

Multi-step reaction with 2 steps

1: triflic azide; copper(ll) sulfate pentahydrate; potassium carbonate / water; methanol / 20 °C / pH 9.5

2: hydrogenchloride / methanol / 4 h / 20 °C

With hydrogenchloride; copper(ll) sulfate pentahydrate; triflic azide; potassium carbonate; In methanol; water;

DOI:10.1039/c4cc03721a

upstream raw materials:

Boc-Lys-OH

dicyclohexylammonium N-tert-butyloxycarbonyl-2-amino-6-azidohexanoate

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