hydrobis(3-phenyl-5-methylpyrazolyl)(3,5-dimethylpyrazolyl)boratothallium

Base Information

• Chemical Name: hydrobis(3-phenyl-5-methylpyrazolyl)(3,5-dimethylpyrazolyl)boratothallium
• CAS No.: 675842-58-7
• Molecular Formula: C₂₅H₂₆BN₆Tl
• Molecular Weight: 625.716
• Mol file: 675842-58-7.mol

Synonyms:

Chemical Property of hydrobis(3-phenyl-5-methylpyrazolyl)(3,5-dimethylpyrazolyl)boratothallium

Chemical Property:

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Useful:

Technology Process of hydrobis(3-phenyl-5-methylpyrazolyl)(3,5-dimethylpyrazolyl)boratothallium

There total 1 articles about hydrobis(3-phenyl-5-methylpyrazolyl)(3,5-dimethylpyrazolyl)boratothallium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thallium(I) nitrate + sodium hydrobis(3-phenyl,5-methylpyrazolyl)(3,5-dimethylpyrazolyl)borate → hydrobis(3-phenyl-5-methylpyrazolyl)(3,5-dimethylpyrazolyl)boratothallium (675842-58-7)

Guidance literature:

In tetrahydrofuran; water; borate dissolved in THF added to aq. soln. of TlNO3; mixt. stirred for 2h; extd. (CH2Cl2); org. phase washed (H2O); CH2Cl2 removed; dissolved in toluene; left for crystn. from toluene/heptane at 4°C; elem. anal.;

DOI:10.1016/j.molstruc.2003.12.002