Technology Process of potassium [2-(hydroxymethyl)-1,3-butadien-1-yl]trifluoroborate
There total 4 articles about potassium [2-(hydroxymethyl)-1,3-butadien-1-yl]trifluoroborate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydrogen bifluoride; water;
In
methanol;
at 20 ℃;
for 18h;
DOI:10.1002/chem.201101624
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1H-imidazole / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
2: N-iodo-succinimide / acetonitrile / 4 h / 0 °C / Inert atmosphere
3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / dimethyl sulfoxide / 4 h / 50 °C / Inert atmosphere
4: potassium hydrogen bifluoride; water / methanol / 18 h / 20 °C
With
1H-imidazole; N-iodo-succinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium hydrogen bifluoride; water; potassium acetate;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1002/chem.201101624
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / dimethyl sulfoxide / 4 h / 50 °C / Inert atmosphere
2: potassium hydrogen bifluoride; water / methanol / 18 h / 20 °C
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium hydrogen bifluoride; water; potassium acetate;
In
methanol; dimethyl sulfoxide;
DOI:10.1002/chem.201101624
