sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate

Base Information

Chemical Name:sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate
CAS No.:1607820-90-5
Molecular Formula:C₆H₁₃NO₈P*Na
Molecular Weight:281.135
Hs Code.:

Synonyms:

Suppliers and Price of sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate

There total 2 articles about sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1607820-88-1
diethyl [2,3,4-tri-O-benzyl-1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol]5-phosphonate

: 1607820-90-5
sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate

Guidance literature:: diethyl [2,3,4-tri-O-benzyl-1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol]5-phosphonate; With pyridine; trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 29h; Inert atmosphere;

With 10 wt% Pd(OH)2 on carbon; hydrogen; acetic acid; In tetrahydrofuran; water; at 20 ℃; for 22h; under 750.075 Torr;

Reference yield:

: 108713-89-9
(2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentan-1-ol

: 1607820-90-5
sodium [1-(N-benzyloxy-N-formylamino)-1,5-dideoxy-D-ribitol] 5-phosphonate

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine; dmap / 14 h / 20 °C

2.1: N-Bromosuccinimide / water; acetone / 0.5 h / 0 °C

3.1: pyridine / methanol / 24 h / 60 °C

3.2: 0.33 h

4.1: Carbonyldiimidazole / tetrahydrofuran / 0.5 h / 0 °C

4.2: 1 h / 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

6.1: 1H-imidazole; triphenylphosphine; iodine / toluene / 1 h / 80 °C / Inert atmosphere

7.1: 3 h / 150 °C

8.1: pyridine; trimethylsilyl bromide / dichloromethane / 29 h / 20 °C / Inert atmosphere

8.2: 22 h / 20 °C / 750.08 Torr

With pyridine; 1H-imidazole; dmap; N-Bromosuccinimide; Carbonyldiimidazole; trimethylsilyl bromide; tetrabutyl ammonium fluoride; iodine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene;