2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol

Base Information

• Chemical Name: 2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol
• CAS No.: 3310-00-7
• Molecular Formula: C₁₄H₂₄O
• Molecular Weight: 208.344
• Mol file: 3310-00-7.mol

Synonyms:

Chemical Property of 2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol

There total 5 articles about 2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

beta-carotene (7235-40-7) → 2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol (3310-00-7)

Guidance literature:

Multi-step reaction with 5 steps

1: iodine; cis–trans isomerase Dwarf27 / hexane / 0.5 h / 20 °C / Enzymatic reaction

2: carotenoid cleavage dioxygenase CCD₇; oxygen; iron(II) sulfate / aq. phosphate buffer / pH 7.8

3: oxygen; iron(II) sulfate; carotenoid cleavage dioxygenase CCD₈ / aq. phosphate buffer

4: water

5: sodium tetrahydroborate

With sodium tetrahydroborate; carotenoid cleavage dioxygenase CCD₇; carotenoid cleavage dioxygenase CCD₈; cis–trans isomerase Dwarf27; water; iodine; oxygen; iron(II) sulfate; In aq. phosphate buffer; hexane;

DOI:10.1111/febs.13400

Reference yield:

9-cis-β-apo-10'-carotenal (1372138-85-6) → 2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol (3310-00-7)

Guidance literature:

Multi-step reaction with 3 steps

1: oxygen; iron(II) sulfate; carotenoid cleavage dioxygenase CCD₈ / aq. phosphate buffer

2: water

3: sodium tetrahydroborate

With sodium tetrahydroborate; carotenoid cleavage dioxygenase CCD₈; water; oxygen; iron(II) sulfate; In aq. phosphate buffer;

DOI:10.1111/febs.13400

Reference yield:

9-cis-β-carotene (13312-52-2) → 2-Methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-1-ol (3310-00-7)

Guidance literature:

Multi-step reaction with 4 steps

1: carotenoid cleavage dioxygenase CCD₇; oxygen; iron(II) sulfate / aq. phosphate buffer / pH 7.8

2: oxygen; iron(II) sulfate; carotenoid cleavage dioxygenase CCD₈ / aq. phosphate buffer

3: water

4: sodium tetrahydroborate

With sodium tetrahydroborate; carotenoid cleavage dioxygenase CCD₇; carotenoid cleavage dioxygenase CCD₈; water; oxygen; iron(II) sulfate; In aq. phosphate buffer;

DOI:10.1111/febs.13400

upstream raw materials:

9-cis-β-carotene

beta-carotene

9-cis-β-apo-10'-carotenal

2-methyl-4-(2,6,6-trimethyl-1-cyclohexene-1-yl)-3-buten-1-al