3-Fluoro-4-methylbenzohydrazide

Base Information

Chemical Name:3-Fluoro-4-methylbenzohydrazide
CAS No.:953735-01-8
Molecular Formula:C₈H₉FN₂O
Molecular Weight:168.171
Hs Code.:
European Community (EC) Number:868-347-8
Mol file:953735-01-8.mol

Synonyms:3-fluoro-4-methylbenzohydrazide;953735-01-8;SCHEMBL18423953;MFCD09729488;STK504237;AKOS000138659;SB86358;CS-0235114;EN300-152928;G32711;A916709

Suppliers and Price of 3-Fluoro-4-methylbenzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
3-Fluoro-4-methylbenzohydrazide
500mg
$ 126.00

Crysdot
3-Fluoro-4-methylbenzohydrazide 97%
5g
$ 446.00

Total 3 raw suppliers

Chemical Property of 3-Fluoro-4-methylbenzohydrazide

Chemical Property:

XLogP3:0.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:168.06989108
Heavy Atom Count:12
Complexity:174

Purity/Quality:

97% ^*data from raw suppliers

3-Fluoro-4-methylbenzohydrazide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)C(=O)NN)F

Technology Process of 3-Fluoro-4-methylbenzohydrazide

There total 1 articles about 3-Fluoro-4-methylbenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 87808-48-8
methyl 3-fluoro-4-methylbenzoate

: 953735-01-8
3-fluoro-4-methylbenzohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; at 100 ℃; for 18h;

Reference yield:

: 953735-01-8
3-fluoro-4-methylbenzohydrazide

: N-(benzo[d]thiazol-6-yl)-N-(4-(5-(difluoromethyl)-1,3,4-oxadiazol-2-yl)-2-fluorobenzyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran / 0.17 h / 20 °C

1.2: 8 h / Reflux

2.1: Burgess Reagent / tetrahydrofuran / 16 h / Reflux

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / dichloromethane / 24 h

4.1: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With N-Bromosuccinimide; Burgess Reagent; 2,2'-azobis(isobutyronitrile); potassium carbonate; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 953735-01-8
3-fluoro-4-methylbenzohydrazide

: N-(4-(5-(difluoromethyl)-1,3,4-oxadiazol-2-yl)-2-fluorobenzyl)-N-(1,3,4-thiadiazol-2-yl)methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran / 0.17 h / 20 °C

1.2: 8 h / Reflux

2.1: Burgess Reagent / tetrahydrofuran / 16 h / Reflux

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / dichloromethane / 24 h

4.1: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With N-Bromosuccinimide; Burgess Reagent; 2,2'-azobis(isobutyronitrile); potassium carbonate; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;