1-bicyclo<1.1.1>pentyl tert-butyl ketone

Base Information

• Chemical Name: 1-bicyclo<1.1.1>pentyl tert-butyl ketone
• CAS No.: 117633-01-9
• Molecular Formula: C₁₀H₁₆O
• Molecular Weight: 152.236
• Mol file: 117633-01-9.mol

Synonyms:

Chemical Property of 1-bicyclo<1.1.1>pentyl tert-butyl ketone

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-bicyclo<1.1.1>pentyl tert-butyl ketone

There total 1 articles about 1-bicyclo<1.1.1>pentyl tert-butyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl isocyanide (630-18-2) + Bicyclo<1.1.1>pent-1-ylphenylthioether (98585-81-0) → 2,2-dimethylpropiophenone (938-16-9) + 1-bicyclo<1.1.1>pentyl tert-butyl ketone (117633-01-9)

Guidance literature:

With lithium 4,4′-di(tert-butyl)biphenyl; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, -65 to -55 deg C, 45 min, 2.) a) ether, -78 deg C, b) RT, 1 h;

DOI:10.1021/ja00162a022

upstream raw materials:

tert-butyl isocyanide

Bicyclo<1.1.1>pent-1-ylphenylthioether