3-<1-methyl-4-<1-methyl-4-(dichloroacetamido)pyrrole-2-carboxamido>pyrrole-2-carboxamido>propionamidine tetraethylammonium sulfate

Base Information

• Chemical Name: 3-<1-methyl-4-<1-methyl-4-(dichloroacetamido)pyrrole-2-carboxamido>pyrrole-2-carboxamido>propionamidine tetraethylammonium sulfate
• CAS No.: 111793-70-5
• Molecular Formula: C₈H₂₀N*C₁₇H₂₁Cl₂N₇O₃*HO₄S
• Molecular Weight: 669.63
• Mol file: 111793-70-5.mol

Synonyms:

Chemical Property of 3-<1-methyl-4-<1-methyl-4-(dichloroacetamido)pyrrole-2-carboxamido>pyrrole-2-carboxamido>propionamidine tetraethylammonium sulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-<1-methyl-4-<1-methyl-4-(dichloroacetamido)pyrrole-2-carboxamido>pyrrole-2-carboxamido>propionamidine tetraethylammonium sulfate

There total 1 articles about 3-<1-methyl-4-<1-methyl-4-(dichloroacetamido)pyrrole-2-carboxamido>pyrrole-2-carboxamido>propionamidine tetraethylammonium sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichloroacethyl chloride (79-36-7) + 3-<1-methyl-4-(1-methyl-4-aminopyrrole-2-carboxamido)pyrrole-2-carboxamido>propionamidine hydrochloride (97950-75-9) + bis(tetraethylammonium) sulfate (2604-85-5) → 3-<1-methyl-4-<1-methyl-4-(dichloroacetamido)pyrrole-2-carboxamido>pyrrole-2-carboxamido>propionamidine tetraethylammonium sulfate (111793-70-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction; 1.) EtOH, THF, -30 deg C to room temperature, 2.) 2-propanol;

DOI:10.1021/jm00397a012

upstream raw materials:

dichloroacethyl chloride

3-<1-methyl-4-(1-methyl-4-aminopyrrole-2-carboxamido)pyrrole-2-carboxamido>propionamidine hydrochloride

bis(tetraethylammonium) sulfate