bis(3-hydroxy-1-methyl-2(1H)-pyridinethione(-1H))zinc(II)

Base Information

• Chemical Name: bis(3-hydroxy-1-methyl-2(1H)-pyridinethione(-1H))zinc(II)
• CAS No.: 864059-89-2
• Molecular Formula: C₁₂H₁₂N₂O₂S₂Zn
• Molecular Weight: 345.761
• Mol file: 864059-89-2.mol

Synonyms:

Chemical Property of bis(3-hydroxy-1-methyl-2(1H)-pyridinethione(-1H))zinc(II)

Chemical Property:

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Useful:

Technology Process of bis(3-hydroxy-1-methyl-2(1H)-pyridinethione(-1H))zinc(II)

There total 1 articles about bis(3-hydroxy-1-methyl-2(1H)-pyridinethione(-1H))zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

zinc(II) acetate dihydrate (5970-45-6) + 3-hydroxy-1-methylpyridine-2(1H)-thione (79246-92-7) → bis(3-hydroxy-1-methyl-2(1H)-pyridinethione(-1H))zinc(II) (864059-89-2)

Guidance literature:

With NaOH; In methanol; water; ligand suspended in MeOH; dissolved by addition of aq. NaOH and H2O; Zn salt in H2O added dropwise; covered in Al foil; heated to reflux (ca. 95°C) under N2 for 30 min; filtered using fine glass frit; washed with water; dried in vac. oven with heat for ca. 12 h;

DOI:10.1039/b505034k

upstream raw materials:

zinc(II) acetate dihydrate

3-hydroxy-1-methylpyridine-2(1H)-thione