netropsin sulfate

Base Information

Chemical Name:netropsin sulfate
CAS No.:18133-23-8
Molecular Formula:C₁₈H₂₆N₁₀O₃*H₂O₄S
Molecular Weight:528.549
Hs Code.:

Synonyms:

Suppliers and Price of netropsin sulfate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of netropsin sulfate

Chemical Property:

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Technology Process of netropsin sulfate

There total 10 articles about netropsin sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6973-60-0
1-Methyl-2-pyrrolecarboxylic acid

: 18133-23-8
netropsin sulfate

Guidance literature:: Multi-step reaction with 6 steps

1: 43 percent / 1.) 70percent nitric acid, acetic anhydride / 1.) a) -15 deg C, 0.5 h, b) RT, 20 min

2: SOCl₂ / tetrahydrofuran / 0.08 h / Heating

3: Hunig's base / tetrahydrofuran / 0.5 h / Ambient temperature

4: 70 percent / H₂ / 10percent Pd/C / dimethylformamide; methanol / 760 Torr

5: 52 percent / DCC / dimethylsulfoxide / 2 h / Ambient temperature

6: 1.) HCl, 2.) NH₃ / 1.) EtOH, RT, 2 h, 2.) EtOH, RT, 1 h

With hydrogenchloride; thionyl chloride; ammonia; hydrogen; nitric acid; acetic anhydride; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo00220a019

Reference yield:

: 13138-78-8
1-methyl-4-nitro-pyrrol-2-carboxylic acid

: 18133-23-8
netropsin sulfate

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / tetrahydrofuran / 0.08 h / Heating

2: Hunig's base / tetrahydrofuran / 0.5 h / Ambient temperature

3: 70 percent / H₂ / 10percent Pd/C / dimethylformamide; methanol / 760 Torr

4: 52 percent / DCC / dimethylsulfoxide / 2 h / Ambient temperature

5: 1.) HCl, 2.) NH₃ / 1.) EtOH, RT, 2 h, 2.) EtOH, RT, 1 h

With hydrogenchloride; thionyl chloride; ammonia; hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo00220a019

Reference yield:

: 28494-51-1
1-methyl-4-nitro-1H-pyrrole-2-carbonyl chloride

: 18133-23-8
netropsin sulfate

Guidance literature:: Multi-step reaction with 4 steps

1: Hunig's base / tetrahydrofuran / 0.5 h / Ambient temperature

2: 70 percent / H₂ / 10percent Pd/C / dimethylformamide; methanol / 760 Torr

3: 52 percent / DCC / dimethylsulfoxide / 2 h / Ambient temperature

4: 1.) HCl, 2.) NH₃ / 1.) EtOH, RT, 2 h, 2.) EtOH, RT, 1 h

With hydrogenchloride; ammonia; hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo00220a019