Technology Process of C15H21IN2O3
There total 1 articles about C15H21IN2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-(3-dimethylaminopropyl)-N-ethylcarbodiimide;
DOI:10.1021/jo500771g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine; trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / 8 h / 20 °C
2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C
3: lithium bromide / 4 h / 20 °C
4: sodium sulfide / methanol
With
sodium sulfide; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; lithium bromide;
In
tetrahydrofuran; methanol;
1: |Sonogashira Cross-Coupling;
DOI:10.1021/jo500771g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine; trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / 8 h / 20 °C
2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C
3: lithium bromide / 4 h / 20 °C
4: sodium sulfide / methanol
5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice
With
sodium sulfide; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide;
In
tetrahydrofuran; methanol; dichloromethane;
1: |Sonogashira Cross-Coupling;
DOI:10.1021/jo500771g
