Technology Process of C42H52O4P2
There total 6 articles about C42H52O4P2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
titanium(IV) isopropylate;
In
tetrahydrofuran;
at 80 ℃;
for 10h;
Schlenk technique;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1.17 h / -78 °C / Schlenk technique; Inert atmosphere
1.2: -78 - 30 °C / Schlenk technique; Inert atmosphere
2.1: 20% palladium hydroxide-activated charcoal; hydrogen / methanol / 8 h / 40 °C / 10343.2 Torr
3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 10 h / 20 - 30 °C / Schlenk technique; Inert atmosphere
4.1: titanium(IV) isopropylate / tetrahydrofuran / 10 h / 80 °C / Schlenk technique; Inert atmosphere; Sealed tube
With
titanium(IV) isopropylate; di-isopropyl azodicarboxylate; 20% palladium hydroxide-activated charcoal; hydrogen; triphenylphosphine; lithium diisopropyl amide;
In
tetrahydrofuran; methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 20% palladium hydroxide-activated charcoal; hydrogen / methanol / 8 h / 40 °C / 10343.2 Torr
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 10 h / 20 - 30 °C / Schlenk technique; Inert atmosphere
3: titanium(IV) isopropylate / tetrahydrofuran / 10 h / 80 °C / Schlenk technique; Inert atmosphere; Sealed tube
With
titanium(IV) isopropylate; di-isopropyl azodicarboxylate; 20% palladium hydroxide-activated charcoal; hydrogen; triphenylphosphine;
In
tetrahydrofuran; methanol;