CH₃NHCOC₅H₄FeC₅H₄CONHCH₂COOH

Base Information

• Chemical Name: CH₃NHCOC₅H₄FeC₅H₄CONHCH₂COOH
• CAS No.: 1000416-28-3
• Molecular Formula: C₁₅H₁₆FeN₂O₄
• Molecular Weight: 344.15
• Mol file: 1000416-28-3.mol

Synonyms:

Chemical Property of CH₃NHCOC₅H₄FeC₅H₄CONHCH₂COOH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CH₃NHCOC₅H₄FeC₅H₄CONHCH₂COOH

There total 1 articles about CH₃NHCOC₅H₄FeC₅H₄CONHCH₂COOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

CH3NHCOC5H4FeC5H4CONHCH2COOCH3 (1000416-25-0) + sodium hydroxide (1310-73-2) → CH3NHCOC5H4FeC5H4CONHCH2COOH (1000416-28-3)

Guidance literature:

In 1,4-dioxane; water; (Ar), Fe complex dissolved in dioxane/H2O 1:1 v/v, cooled to 10°C, treated with NaOH, stirred at room temp. for 10 min; treated with concd.HCl to pH=2-3, extd.(EtOAc), washed (satd. aq.NaHCO3,H2O), org. layer dried (Na2SO4), evapd.(vac.);

DOI:10.1002/ejic.200601230

upstream raw materials:

CH₃NHCOC₅H₄FeC₅H₄CONHCH₂COOCH₃

sodium hydroxide