sparteine-10,17-dione

Base Information

Chemical Name:sparteine-10,17-dione
CAS No.:52345-93-4
Molecular Formula:C₁₅H₂₂N₂O₂
Molecular Weight:262.352
Hs Code.:

Synonyms:

Suppliers and Price of sparteine-10,17-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of sparteine-10,17-dione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of sparteine-10,17-dione

There total 48 articles about sparteine-10,17-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: (+/-)-Δ^3,13-didehydro-10,17-dioxo-β-isosparteine

: 489-54-3,52717-73-4,52717-74-5,52717-75-6,52345-93-4
(+/-)-10,17-dioxo-β-isosparteine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; water; for 7h;

Reference yield: 81.0%

: (1R,4S,5R,8S)-4,8-bis(4-chlorobutyl)-3,7-diazabicyclo[3.3.1]nonane-2,6-dione

: 52345-93-4
(+)-10,17-dioxo-β-isosparteine

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; potassium hydroxide; In dimethyl sulfoxide; at 60 ℃; for 4h;
DOI:10.1021/acs.orglett.7b01475

Reference yield:

: (+/-)-(1R,4S,5R,8S,)-2,6-dioxo-3,4,7,8-tetraallyl-3,7-diazabicyclo[3.3.1]nonane

: 489-54-3,52717-73-4,52717-74-5,52717-75-6,52345-93-4
(+/-)-10,17-dioxo-β-isosparteine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / (Cy₃P)2Cl₂Ru=CHPh / CH₂Cl₂ / 16 h / Heating

2: 94 percent / H₂ / Pd/C / methanol; H₂O / 7 h

With Grubbs catalyst first generation; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; water;