4-amino-5--1-methyl-2-methoxy-6-oxopyrimidine

Base Information

Chemical Name:4-amino-5--1-methyl-2-methoxy-6-oxopyrimidine
CAS No.:137512-95-9
Molecular Formula:C₁₈H₂₅N₅O₁₁
Molecular Weight:487.423
Hs Code.:

4-amino-5-<N-nitroso-β-D-(3,4,5-tri-O-acetyl)glucopyranosylamino>-1-methyl-2-methoxy-6-oxopyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-amino-5--1-methyl-2-methoxy-6-oxopyrimidine

Chemical Property:

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Technology Process of 4-amino-5--1-methyl-2-methoxy-6-oxopyrimidine

There total 2 articles about 4-amino-5--1-methyl-2-methoxy-6-oxopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 108-24-7
acetic anhydride

: 137512-94-8
4-amino-5-(N-nitrosoglucopyranosylamino)-1-methyl-2-methoxy-6-oxopyrimidine

: 137512-95-9
4-amino-5--1-methyl-2-methoxy-6-oxopyrimidine

Guidance literature:: In pyridine; for 7h; Ambient temperature;
DOI:10.1002/jhet.5570280538

Reference yield:

: 85357-28-4
4-amino-1,6-dihydro-5-glucosylamino-1-methyl-2-methoxy-6-oxopyrimidine

: 137512-95-9
4-amino-5--1-methyl-2-methoxy-6-oxopyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / sodium nitrite, 1N HCl / H₂O / 0.25 h / Ambient temperature

2: 52 percent / pyridine / 7 h / Ambient temperature

With hydrogenchloride; sodium nitrite; In pyridine; water;
DOI:10.1002/jhet.5570280538