C₁₂H₁₅BrN₄O₄

Base Information

• Chemical Name: C₁₂H₁₅BrN₄O₄
• CAS No.: 1637533-84-6
• Molecular Formula: C₁₂H₁₅BrN₄O₄
• Molecular Weight: 359.179

Synonyms:

Chemical Property of C₁₂H₁₅BrN₄O₄

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl2-(8-bromo-7-methyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-1-yl)acetate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₂H₁₅BrN₄O₄

There total 6 articles about C₁₂H₁₅BrN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C14H21BrN4O5 → C12H15BrN4O4 (1637533-84-6)

Guidance literature:

With potassium tert-butylate; In 1,4-dioxane; at 20 ℃; for 1h;

Reference yield:

4-amino-1-methylimidazole-5-carboxylate ethyl ester (61982-18-1) → C12H15BrN4O4 (1637533-84-6)

Guidance literature:

Multi-step reaction with 6 steps

1: acetic acid / 10 h / 110 °C

2: N-Bromosuccinimide / dichloromethane / 20 h / 20 °C

3: hydrazine hydrate / ethanol / 2 h / 80 °C

4: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

5: dichloromethane / 1 h / 0 °C

6: potassium tert-butylate / 1,4-dioxane / 1 h / 20 °C

With N-Bromosuccinimide; potassium tert-butylate; hydrazine hydrate; acetic acid; triethylamine; In 1,4-dioxane; ethanol; dichloromethane;

Reference yield:

C15H13N3O4 → C12H15BrN4O4 (1637533-84-6)

Guidance literature:

Multi-step reaction with 5 steps

1: N-Bromosuccinimide / dichloromethane / 20 h / 20 °C

2: hydrazine hydrate / ethanol / 2 h / 80 °C

3: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

4: dichloromethane / 1 h / 0 °C

5: potassium tert-butylate / 1,4-dioxane / 1 h / 20 °C

With N-Bromosuccinimide; potassium tert-butylate; hydrazine hydrate; triethylamine; In 1,4-dioxane; ethanol; dichloromethane;

upstream raw materials:

4-amino-1-methylimidazole-5-carboxylate ethyl ester

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