triphenylene-1,5,9-triamine

Base Information

Chemical Name:triphenylene-1,5,9-triamine
CAS No.:371786-11-7
Molecular Formula:C₁₈H₁₅N₃
Molecular Weight:273.337
Hs Code.:

Synonyms:

Suppliers and Price of triphenylene-1,5,9-triamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of triphenylene-1,5,9-triamine

Chemical Property:

Boiling Point:631.0±50.0 °C(Predicted)
Density:1.376±0.06 g/cm3(Predicted)

Purity/Quality:: 99.0% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of triphenylene-1,5,9-triamine

There total 2 articles about triphenylene-1,5,9-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1,5,9-trinitrotriphenylene

: 371786-11-7
triphenylene-1,5,9-triamine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; ethyl acetate; at 20 ℃; under 760.051 Torr;
DOI:10.1039/c5cc08853d

Reference yield:

: 3209-22-1
1,2-Dichloro-3-nitrobenzene

: 371786-11-7
triphenylene-1,5,9-triamine

Guidance literature:: Multi-step reaction with 2 steps

1: copper / N,N-dimethyl-formamide / 12 h / Reflux; Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethyl acetate; ethanol / 20 °C / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; copper; In ethanol; ethyl acetate; N,N-dimethyl-formamide; 1: |Ullmann Condensation;
DOI:10.1039/c5cc08853d

Reference yield:

: 371786-11-7
triphenylene-1,5,9-triamine

: 2,6,10-triphenyl-1,5,9-triazocoronene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 22 h / 20 °C / Inert atmosphere

2: sodium chloride; aluminum (III) chloride / 4 h / 220 °C / Sealed tube; Inert atmosphere

With aluminum (III) chloride; triethylamine; sodium chloride; In tetrahydrofuran;
DOI:10.1039/c5cc08853d